Sumitomo Chemical Company, Limited

Masatoshi Uegaki

Yuzo Maegawa

Norio Kotera

Takashi Miyaoka

Tatsuo Kaneoya

Shinzaburo Masaki

Masakatsu Yoshimura

Akira Fukasawa

Masatoshi Takahashi

A method for purifying 1-aminoanthraquinone which comprises previously subjecting a crude 1-aminoanthraquinone to a removal treatment of inorganic impurities so that their content is reduced to not more than 4 wt. % as converted to ash basis or to a removal treatment of iodine-consuming reductive inorganic impurities so that their content is reduced to not more than 2 wt. % as converted to consumed iodine basis, and then rectifying the 1-aminoanthraquinone.

Method for purifying 1-aminoanthraquinone

A high melting, high boiling organic compound is easily and stably purified by continuously supplying the molten organic compound to a rectification zone under a subatmospheric pressure and continuously distilling off and recovering vapors from the top of the rectification zone, while continuously withdrawing bottoms containing higher boiling impurities and/or involatile impurities than the desired compound from a reboiling zone at the bottom of the rectification zone to the outside of rectification system by means of a barometric leg, without any pretreatment of removing lower boiling impurities therefrom before the rectification, and without disturbing a pressure balance in the rectification system.

Purification of compounds having high melting point

Growing community of inventors

Nara, Japan

Masatoshi Uegaki