Fuji Photo Film Company, Limited

Masatoshi Kiyama

Shinichi Funabashi

Hiroshi Ogawa

Chiaki Mizuno

Takao Komi

Masaaki Fujiyama

Yasuyuki Yamada

Kiyomi Ejiri

Akihiro Matsufuji

Nobuo Tsuji

Mikio Ohno

Kunihiko Honda

Koichi Yamauchi

A method of preparing a magnetic coating composition comprises a first process for kneading ferromagnetic grains, a binder and a binder solution Y1 by use of a two-shaft continuous kneading and mixing machine to obtain a kneaded mixture K1 having a solid content within the range of 65 wt % to 95 wt %, a second process for kneading a binder solution Y2 and the kneaded mixture K1 by use of the two-shaft continuous kneading and mixing machine to obtain a primary diluted mixture K2 having a solid content within the range of 50 wt % to 70 wt %, a third process for diluting and dispersing the primary diluted mixture K2 in an organic solvent to obtain a secondary diluted mixture K3 having a solid content within the range of 25 wt % to 50 wt %, and a fourth process for finely dispersing the secondary diluted mixture K3 to obtain a dispersion mixture K4 having a solid content within the range of 25 wt % to 45 wt %.

Method of preparing magnetic coating composition

A method for making a magnetic recording medium comprises the steps of mixing ferromagnetic grains and a surface treating agent, grinding the resulting mixture, and thus obtaining a ground mixture. A binder and a solvent are added to the ground mixture, which results from the mixing and grinding process, the resulting mixture is kneaded and diluted, and a kneaded and diluted mixture is thus obtained. An additive and a solvent are then added to the kneaded and diluted mixture, which results from the kneading and diluting process, a dispersion process is carried out on the resulting mixture, and a dispersion mixture is thereby obtained. Thereafter the dispersion mixture, which results from the dispersion process, is applied to a non-magnetic substrate.

Method for making magnetic recording media

A method of preparing a kneaded mixture for a magnetic coating material comprises a kneading start process and a continuous kneading process. In the kneading start process, a low-viscosity composition, which is composed of magnetic layer forming materials containing ferromagnetic grains and a binder, and a solvent, is introduced into a kneading vessel of a two-shaft continuous kneading and mixing machine, and kneading is started. In the continuous kneading process, after the start of the kneading, a high-viscosity composition, in which a solvent amount is smaller by at least 7 wt % than the solvent amount in the low-viscosity composition used in the kneading start process, is continously introduced into the kneading vessel, and the kneading is continued while high shearing force is being given to the high-viscosity composition.

Method of preparing kneaded mixture for magnetic coating material

A magnetic recording medium which comprises a non-magnetic support having thereon a magnetic recording layer containing a ferromagnetic fine powder and a binder as main components is disclosed. The magnetic recording layer containing as the binder (1) a vinyl chloride-vinyl acetate-maleic acid copolymer which has a mean polymerization degree of about 300 to about 400 and a maleic acid fraction of about 0.6 to about 1.5 wt %, (2) a polyurethane resin which has a number average molecular weight of 40,000 to 100,000 and is prepared from (i) a mixture of polyneopentyladipate having a mean molecular weight of 500 to 2,500 and polybutyleneadipate having a mean molecular weight of 500 to 2,500 with a mixing ratio of the former to the latter of from 2/8 to 9/1 by weight and (ii) diphenylmethane diisocyanate, and optionally (3) a low molecular weight polyisocyanate compound.

Magnetic recording medium

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Kanagawa, Japan

Masatoshi Kiyama