The Boc Group, Inc.

Mary Kristin Nicholes

Mark R Litchy

Donald Clarke Grant

Stephen Carlson

A dilution apparatus for continuously producing a diluted liquid sample, e.g., a chemical-mechanical polishing slurry, for analysis, e.g., particle size distribution, comprises a mixer manifold, a diluent-introducing means, e.g., a flow controlling device, for introducing a diluent, e.g., water, into the mixer manifold, and a liquid sample introducing means, e.g., a pump, for introducing the sample into the mixer manifold. The mixer manifold includes a plurality of ports for receiving a plurality of liquid samples from a plurality of sample points. The dilution apparatus can include a second mixer manifold for continuously producing a second diluted liquid sample, and it can be associated with one or more sensors operable to measure sample properties, e.g., an optical particle counter. The sensors can be operated simultaneously, and the measurements of the sensors can be compared. The dilution apparatus is capable of improving accuracy, reliability, repeatability, sensitivity and versatility of the associated sensors, and it is less complex than conventional dilution systems.

Dilution apparatus and method of diluting a liquid sample

An apparatus and method for drawing a sample of a chemical-mechanical polishing slurry for analysis of at least one property, e.g., particle size distribution, is described. The apparatus comprises (i) a plurality of sample delivery lines, each line carrying a chemical-mechanical polishing slurry, (ii) a manifold in fluid communication with the plurality of sample delivery lines, (iii) means for opening and closing the fluid communication between each sample delivery line and the manifold, (iv) an aspirator in fluid communication with the manifold, (vi) means opening and closing the fluid communication between the aspirator and the manifold, (vii) a pressure between the aspirator and the sample delivery lines, a reduction in the pressure resulting in the draw of a sample from the sample delivery line into the manifold when the fluid communication between the line and the manifold is open, (viii) a sensor for measuring the at least one property of the slurry, the sensor in fluid communication with the manifold, and (ix) means for opening and closing the fluid communication between the manifold and the sensor.

Growing community of inventors

Eden Prairie, MN, United States of America

Mary Kristin Nicholes