Heraeus Quarzglas Gmbh & Co Kg

Shin-etsu Quartz Products Ltd.

Heraeus Battery Technology Gmbh

Martin Trommer

Michael Hünermann

Stefan Ochs

Kay Schuster

Walter Lehmann

Manuel Rosenberger

Steffen Weimann

Jan Vydra

Andreas Langner

Stephan Thomas

Klaus Becker

Michael Huenermann

Thomas Kayser

Bruno Uebbing

Bodo Kühn

Hilmar Laudahn

Akira Fujinoki

Waltraud Werdecker

Hiroyuki Nishimura

Matthias Otter

Jörg Becker

Oliver Ganz

Bodo Kuehn

Nigel Robert Whippey

Ralph Sattmann

Jürgen Weber

Helmut Leber

Tetsuji Ueda

Ian George Sayce

Sascha Pihan

Nils Christian Nielsen

Udo Peper

Juergen Weber

Dominik Samuelis

Mario Such

Steffen Zwarg

Gerhard Schötz

Norbert Otto

Malte Schwerin

Martin Thürer

Mirko Wittrin

Norbert Traeger

Stefan Hengster

Klaus-Uwe Badeke

Stephan Grimm

Rene Sowa

Steffen Kaiser

Wolfgang Stang

Enrico Ehrentraut

Frank Froehlich

Johannes Kirchhof

Joerg Becker

Rainer Berg

Ulrich Kirst

David Kostka

Yusuf Tansel

Andreas Brueckel

Ralph Sattman

Anke Schuster

Tobias Pogge

Gero Fischer

Ulla Holst

Michael HÜNERMANN

Achim Hofmann

Frank Wessely

André Kalide

Martin Leich

Florian Just

A method for homogenizing glass includes the method: providing a cylindrical blank composed of the glass having a cylindrical outer surface that extends along a longitudinal axis of the blank between a first end face and a second end face, forming a shear zone in the blank by softening a longitudinal section of the blank and subjecting it to a thermal-mechanical intermixing treatment, and displacing the shear zone along the longitudinal axis of the blank. The displacement of the shear zone along the longitudinal axis of the blank is superimposed by a simultaneous oscillating motion of the shear zone along the longitudinal axis of the blank. The first end of the blank is rotated at a first rotational speed and the second end of the blank is rotated at a second rotational speed. An oscillating motion of the shear zone is generated by periodically varying the first and/or second rotational speed.

Method for homogenizing glass

Described is a process for the production of synthetic fused silica in which the deposition surface is located for a period of at least 50% of the build-up time of the soot body at a burner distance in which the horizontally integrated luminous intensity of the flame of the burner used in the targetless state is still at least ⅔ of the maximum horizontally integrated luminous intensity of the flame.

Process for the preparation of synthetic quartz glass

Methods are known for producing an anti-resonant hollow-core fiber which has a hollow core extending along a fiber longitudinal axis and an inner jacket region that surrounds the hollow core, said jacket region comprising multiple anti-resonant elements. The known methods have the steps of: providing a cladding tube that has a cladding tube inner bore and a cladding tube longitudinal axis along which a cladding tube wall extends that is delimited by an interior and an exterior; providing a number of tubular anti-resonant element preforms; arranging the anti-resonant element preforms at target positions of the interior of the cladding tube wall, thereby forming a primary preform which has a hollow core region and an inner jacket region; and elongating the primary preform in order to form the hollow-core fiber or further processing the primary preform in order to form a secondary preform. The aim of the invention is to achieve a high degree of precision and an exact positioning of the anti-resonant elements in a sufficiently stable and reproducible manner on the basis of the aforementioned methods. This is achieved in that while carrying out a process according to step (c), components of the primary preform made of quartz glass and/or parts surrounding the primary preform made of quartz glass are heated and softened together, wherein the quartz glass of at least one of the preform components and/or the quartz glass of at least one of the parts surrounding the preform contains at least one dopant which decreases or increases the viscosity of quartz glass.

Methods for producing a hollow-core fiber and for producing a preform for a hollow-core fiber

Methods are known for producing an anti-resonant hollow-core fiber which has a hollow core extending along a fiber longitudinal axis and an inner jacket region that surrounds the hollow core, said jacket region comprising multiple anti-resonant elements. The known methods have the steps of: providing a cladding tube that has a cladding tube inner bore and a cladding tube longitudinal axis along which a cladding tube wall extends that is delimited by an interior and an exterior; providing a number of tubular anti-resonant element preforms; arranging the anti-resonant element preforms at target positions of the interior of the cladding tube wall, thereby forming a primary preform which has a hollow core region and an inner jacket region; and elongating the primary preform in order to form the hollow-core fiber or further processing the primary preform in order to form a secondary preform. The aim of the invention is to achieve a high degree of precision and an exact positioning of the anti-resonant elements in a sufficiently stable and reproducible manner on the basis of the aforementioned methods. This is achieved in that a secondary preform is formed which has an outer diameter ranging from 30 to 90 mm, and at least one of the end faces of the anti-resonant element preforms is closed prior to drawing the fiber.

Methods are known for producing an anti-resonant hollow-core fiber which has a hollow core extending along a fiber longitudinal axis and an inner jacket region that surrounds the hollow core, said jacket region comprising multiple anti-resonant elements. The known methods have the steps of: providing a cladding tube that has a cladding tube inner bore and a cladding tube longitudinal axis along which a cladding tube wall extends that is delimited by an interior and an exterior; providing a number of tubular anti-resonant element preforms; arranging the anti-resonant element preforms at target positions of the interior of the cladding tube wall, thereby forming a primary preform which has a hollow core region and an inner jacket region; and further processing the primary preform in order to form a secondary preform, including a process of elongating the primary preform in order to directly form the hollow-core fiber or to form the secondary preform. The aim of the invention is to achieve a high degree of precision and an exact positioning of the anti-resonant elements in a sufficiently stable and reproducible manner on the basis of the aforementioned methods. This is achieved in that a primary preform with an outer diameter ranging from 20 to 70 mm is used for the elongation process.

Methods are known for producing an anti-resonant hollow-core fiber which has a hollow core extending along a fiber longitudinal axis and an inner jacket region that surrounds the hollow core, said jacket region comprising multiple anti-resonant elements. The known methods have the steps of: providing a cladding tube that has a cladding tube inner bore and a cladding tube longitudinal axis along which a cladding tube wall extends that is delimited by an interior and an exterior; providing a number of tubular anti-resonant element preforms; arranging the anti-resonant element preforms at target positions of the interior of the cladding tube wall, thereby forming a primary preform which has a hollow core region and an inner jacket region; and elongating the primary preform in order to form the hollow-core fiber or further processing the primary preform in order to form a secondary preform. The aim of the invention is to achieve a high degree of precision and an exact positioning of the anti-resonant elements in a sufficiently stable and reproducible manner on the basis of the aforementioned methods. This is achieved in that while further processing the primary preform according to step (c), an external layer cylinder is used which has a radial viscosity profile such that the viscosity increases towards the interior of the external layer cylinder.

Described is a method of producing synthetic fused silica in which the synthetic flame used in the method has a ratio of the Full Width at Half Maximum (FWHM) vertical luminous intensity to the Full Width at Half Maximum (FWHM) horizontal luminous intensity greater than 10 in a targetless state, the luminous intensities being measured in candela/mm.

A process for the production of a fluorinated quartz glass including the steps of generating SiOparticles in a synthesis burner; depositing the resulting SiOparticles into a body; and vitrifying the resulting body, wherein a fluorinating agent having a boiling point greater than or equal to −10° C. is supplied to the synthesis burner.

Process for the preparation of fluorinated quartz glass

Methods are known for producing an anti-resonant hollow-core fiber which has a hollow core extending along a fiber longitudinal axis and an inner jacket region that surrounds the hollow core, said jacket region comprising multiple anti-resonant elements. The known methods have the steps of: providing a cladding tube that has a cladding tube inner bore and a cladding tube longitudinal axis along which a cladding tube wall extends that is delimited by an interior and an exterior; providing a number of tubular anti-resonant element preforms; arranging the anti-resonant element preforms at target positions of the interior of the cladding tube wall, thereby forming a primary preform which has a hollow core region and an inner jacket region; further processing the primary preform in order to form a secondary preform, including an elongation process; and drawing the secondary preform in order to form the hollow-core fiber. The aim of the invention is to achieve a high degree of precision and an exact positioning of the anti-resonant elements in a sufficiently stable and reproducible manner on the basis of the aforementioned methods. This is achieved in that after the primary preform is elongated, at least some of the formerly tubular anti-resonant element preforms of the primary preform have an oval outer cross-sectional shape with a longest cross-sectional axis Aand a shortest cross-sectional axis A, wherein the ratio A/Aof the length of the axes ranges from 1.01 to 1.27, and the shortest cross-sectional axis Aruns in a radial direction when viewed from the cladding tube longitudinal axis.

A process for producing a fluorinated quartz glass is described, including providing an SiOsoot body; reacting the SiOsoot body with a fluorinating agent having a boiling point of greater than or equal to −10° C. to obtain a fluorinated SiOsoot body; and vitrifying the fluorinated SiOsoot body.

Alternative fluorinating agents for the production of fluorinated quartz glass

A method for homogenizing glass includes the method: providing a cylindrical blank composed of the glass having a cylindrical outer surface that extends along a longitudinal axis of the blank between a first end face and a second end face, forming a shear zone in the blank by softening a longitudinal section of the blank and subjecting it to a thermal-mechanical intermixing treatment, and displacing the shear zone along the longitudinal axis of the blank. To enable a radial mixing within the shear zone in addition to the tangential mixing with the lowest possible time and energy input, starting from this method, cylindrical sections of the blank are adjacent to the shear zone on both sides, the first cylindrical section having a first central axis and the second cylindrical section having a second central axis, the first central axis and the second central axis being temporarily non-coaxial with each other.

A known method for homogenizing glass includes the following steps: providing a cylindrical blank composed of the glass, having a cylindrical outer surface which extends between a first end face and a second end face, forming a shear zone in the blank by softening a longitudinal section of the blank and subjecting it to a thermal-mechanical intermixing treatment, and moving the shear zone along the longitudinal axis of the blank. To reduce the risk of cracks and fractures during homogenizing, it is proposed that a thermal radiation dissipator is used that at least partially surrounds the shear zone, the lateral dimension of which in the direction of the longitudinal axis of the blank is greater than the shear zone and smaller than the length of the blank, the thermal radiation dissipator being moved synchronously with the shear zone along the longitudinal axis of the blank.

Method and device for homogenizing glass

A method for the production of synthetic quartz glass using a special cleaning device is provided. The method includes (a) evaporating a production material containing a polymerizable polyalkylsiloxane compound while forming a production material vapor, (b) passing the production material vapor resulting from step (a) through a cleaning device to purify the production material vapor, (c) supplying the purified production material vapor resulting from step (b) to a reaction zone in which the purified production material vapor is converted to SiOparticles through oxidation and/or through hydrolysis, (d) depositing the SiOparticles resulting from step (c) on a deposition surface, and optionally drying and vitrifying the deposited SiOparticles resulting from step (d) to form synthetic quartz glass. The cleaning device includes a bulk of porous silica particles which have a BET specific surface area of at least 2 m/g. A device for carrying out the method is also provided.

Process for producing synthetic quartz glass using a cleaning device

A method for producing synthetic fused quartz is provided. The method includes evaporating a feedstock material which contains at least one polymerizable polyalkylsiloxane compound, and supplying the feedstock material vapor to a reaction zone, wherein the feedstock material vapor is converted by oxidation and/or by hydrolysis into SiOparticles. The feedstock material vapor is passed through a membrane filter as a cleaning device to reduce the formation of gel, which is typically associated with the production of synthetic fused quartz.

Method and apparatus for producing fused quartz from a polymerizable polyalkylsiloxane compound with membrane filter as cleaning device

A method for manufacturing quartz glass, wherein (a) an appropriate liquid starting material is evaporated by spraying it into a vertically arranged evaporation chamber, (b) the vaporous starting material is oxidized to form SiO, and the SiOis collected. The method is characterized in that the starting material to be evaporated is sprayed in on the bottom of the evaporation chamber and the vaporous starting material is removed at the top end of the evaporation chamber, wherein the evaporation chamber is designed such that components depositing in the chamber accumulate on the bottom of the evaporator and are sprayed once again, as well as an evaporator for applying the method.

Evaporator and method for producing synthetic fused quartz

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Bitterfeld, Germany

Martin Trommer