Fmc Corporation

Cogas Development Company

Martin E Sacks

James L Manganaro

James Carmichael

Richard H McClelland

This invention relates to a process for producing Caro's acid by reaction of at least 85% by weight sulfuric acid and at least 50% by weight hydrogen peroxide wherein the sulfuric acid and hydrogen peroxide are fed through separate feed lines into a funneling zone open to the atmosphere, the feed lines having air gaps between their ends and the funneling zone; passing said hydrogen peroxide and sulfuric acid by gravity flow from said funneling zone into one end of a reaction zone whose size permits a pressure drop which is at least 8 times the theoretical pressure drop for such reaction zone and removing a mixture containing Caro's acid from the exit end of the reaction zone.

Method for producing caro's acid

This invention relates to a process for producing Caro's acid by reaction of at least 85% by weight sulfuric acid and at least 50% by weight hydrogen peroxide wherein the sulfuric acid and hydrogen peroxide are fed through separate feed lines into a funneling zone open to the atmosphere, the feed lines having air gaps between their ends and the funneling zone; continuing to introduce the sulfuric acid and the hydrogen peroxide into the funneling zone to flow and mix within the funneling zone, passing the resulting mixture by gravity flow into one end of a reaction zone whose size permits a pressure drop which is at least 8 times the theoretical pressure drop for such reaction zone and removing a mixture containing Caro's acid from the exit end of the reaction zone.

Method for producing Caro's acid

In a system of fluidized gasification of carbonaceous solids in which fines are burned in an external combustor to heat recycle solids, fines entrainment is reduced by introducing the finest of the fines into the combustor from the lower end of a fluidized fines feeder vessel whereby the said finest fines are selectively burned.

Gasification of carbonaceous solids

Coal gasification process gives a waste water stream containing phenolic impurities. This stream is fed into contact with hot solid heat transfer particles to form superheated steam which is fed to the gasification zone.

Growing community of inventors

East Windsor, NJ, United States of America

Martin E Sacks