Pcr, Inc.

Brevets, LLC

Other

Archimica (florida), Inc.

Continuous Extractions, LLC

Es Industries

Mark A Buese

Rudy Strohschein

John Scott Shaffer

Gary E LeGrow

Benigno A Janeiro

A closed couplable extractor has a plurality of tubes that function as extracting chamber tubes and/or solution receiver tubes where the tubes are fixed or reversibly connected. Tubes from two closed couplable extractors can be placed in proximal contact to exchange heat between tubes in coupled extractors. Adjacent pairs of tubes in an extractor are connected by at least two transfer conduits, allowing positioning the pair of tubes a higher and lower tubes for distilling vapor through vapor conduits to higher tubes and draining extract solution through solution conduits to lower tubes. The extractor has at least one valve to isolate the extractor from ambient and optional valves to isolate tubes within the extractor. Valves can be couplable valves that permit one or more tubes to enter and exit the system without removal of air or loss of liquid to the environment during these steps while performing extraction processes.

Couplable closed extractors and methods for their use

Continuous extraction units (CEUs) are constructed that allow switching of extraction chambers (ECs) that contain extractable material (EM) and extract solution. Extraction chambers can be removable and replaceable, where the CEU has a fluid flow portion and a liquid transfer portion. Quick-connect valves allow exchange of ECs in the CEU while under flow without solvent loss. Alternatively, the CEU employs pairs of ECs where a first EC at equilibrium partitioning of an extract solution drains to an expansion chamber (EXC) with an expansion valve (EV) and a heat transfer tube situated proximal to or shared with a solvent condenser (SC) to form of a double phase change heat exchanger (HE). Solvent from the SC fills a paired EC containing EM. A second pair of ECs has a first EC with EM and solvent establishing equilibrium and a second EC that is emptied of spent EM, filled with fresh EM, and readied to receive solvent.

Continuous extraction unit and double phase change heat exchanger and method for continuous extraction

Continuous extraction concentration and isolation units are constructed with at least one extraction chambers containing extractable material. Without disruption of total fluid flow in the unit: an extraction chamber completely depleted of extract can be refilled with fresh extractable material or can be replaced with an extraction chamber containing fresh extractable material. Extract are continuously separated from one or more solvents in expansion chambers and removed. All solvents can be retained within the unit. One or more compressors circulate the fluids through the extraction chambers, the expansion chamber, and a condenser, where the expansion chamber and the condenser can be coupled as a heat exchanger. One or more isolators can be included for selectively removing components that are extracted from the plant material without disruption of the process and provide the removed components in concentrated or pure form.

Continuous extractor, concentrator, dryer, and isolator

Extraction units are constructed having at least one extraction chamber containing extractable material. The extract is continuously separated from the solvent in an expansion chamber where it is continuously or periodically removed from the unit. One or more means for fluid flow can be used to circulate the fluid through the extraction chambers and the expansion chamber, where the expansion chamber and a condenser or the output of the means for fluid flow are coupled as a heat exchanger.

Extractor and concentrator

Continuous extraction units are constructed having a plurality of extraction chambers containing extractable material. Without disruption of total fluid flow in the unit: an extraction chamber completely depleted of extract can be evacuated of solvent and replaced with an extraction chamber containing fresh extractable material. The extract is continuously separated from the solvent in an expansion chamber where it is continuously or periodically removed from the unit. All solvent can be retained within the unit. One or more compressors can be used to circulate the fluid through the extraction chambers, the expansion chamber, and a condenser, where the expansion chamber and the condenser can be coupled as a heat exchanger.

Continuous extractor, concentrator and dryer

Alkylmethylsiloxane-dimethylsiloxane polyalkylene oxide copolymers useful as surfactants for both oil-in-water emulsions and silicone-in-water emulsions are disclosed.

Alkylmethylsiloxane-dimethylsilicone polyalkylene oxide copolymers

Compositions of unstrained perfluorinated organo substituted cyclosiloxanes of formula (I): ##STR1## wherein m is an integer of 1 to 12; n is an integer of 1 to 4; X is a divalent radical which may include O, NH, N(CH.sub.3), OC(O), NHC(O), N(CH.sub.3)C(O)CH.sub.2 ; and R.sup.F is a perfluorinated straight chain or branched chain monovalent alkyl radical of 1 to 25 carbon atoms; or R.sup.F is a perfluorinated ether radical of the general formula (II): ##STR2## wherein p is an integer of 1 to 10 are described, along with copolymer compositions prepared from these cyclopolysiloxanes and from mixtures of these cyclosiloxanes and other siloxanes.

Perfluorinated organo substituted cyylosiloxanes and copolymers prepared

The invention provides high purity 3-aminopropylmethylsiloxanes of the general formulae: ##STR1## wherein each R may be the same or different aryl group, or monovalent straight or branched chain alkyl group having from 1 to about 18 carbon atoms, Me is methyl, and x may range from about 3 to about 5, the process comprising

Aminoorganofunctionalsiloxanes

Compositions of unstrained perfluorinated ether organo substituted cyclosiloxanes of formula (I): ##STR1## wherein m is an integer of 1 to 12; n is an integer of 1 to 4; X is a divalent radical which may include O, NH, N(CH.sub.3), OC(O), NHC(O), N(CH.sub.3)C(O)CH.sub.2 ; and R.sup.F is a perfluorinated ether radical of the general formula (II): ##STR2## wherein p is an integer of 1 to 10 are described, along with copolymer compositions prepared from these cyclopolysiloxanes and from mixtures of these cyclosiloxanes and other siloxanes.

Perfluorinated ether organo substituted cyclosiloxanes and copolymers

Compositions of Formula (I): ##STR1## wherein R is a group selected in accordance with an intended application; R.sub.1 and R.sub.2 are protecting groups; and P is a substrate are provided. Methods of producing these compositions are also provided.

Growing community of inventors

Gainesville, FL, United States of America

Mark A Buese