Matsushita Electric Industrial Co., Ltd.

Panasonic Corporation

Ricoh Company, Ltd.

Matsushita Electrical Industrial Co., Ltd.

Mamoru Soga

Kazufumi Ogawa

Norihisa Mino

Hidekazu Arase

Masaichiro Tatekawa

Nobuo Sonoda

Shigeo Ikuta

Shu Hotta

Tohru Nakagawa

Hiroyuki Matsuo

Wataru Shimotsuma

Shinji Ozaki

Yasuhito Yuasa

Tsutomu Matsuda

Yoshio Kishimoto

Keishi Taniguchi

Takaiki Nomura

Yasuo Takebe

Keiichi Yubakami

Takamichi Enomoto

Shigeru Kusakata

Masashi Ito

Tsuneo Shibata

Masashi Itoh

Kenji Tomita

Tadashi Otake

Tadashi Ootake

Keisuke Shimamoto

Yusuke Mochizuki

Hidetaka Higashino

Susumu Maruno

Yoshikazu Yamagata

Katsuya Wakita

Masahisa Maeda

Tokihiko Shimizu

Yoichi Sekine

Takuma Takasu

Ogawa Kazufumi

Takatoshi Minoda

Kazuo Akagi

Hideki Shirakawa

A toner or two-component developer is provided. The toner includes toner base particles obtained by mixing in an aqueous medium a first resin particle dispersion, a colorant particle dispersion, and a wax particle dispersion, aggregating the mixed dispersion to form core particles at least part of which is melted, adding a second resin particle dispersion to a core particle dispersion in which the core particles are dispersed, and fusing the second resin particles with the core particles by heating. A GPC measurement of the second resin particles shows that the number-average molecular weight (Mn2) is 9000 to 30000, the weight-average molecular weight (Mw2) is 50000 to 500000, and the ratio (Mw2/Mn2) of the weight-average molecular weight (Mw2) to the number-average molecular weight (Mn2) is 2 to 10. The wax particles include at least a first wax and a second wax. An endothermic peak temperature (melting point Tmw1) of the first wax based on a DSC method is 50&#xb0; C. to 90&#xb0; C. The relationship between an endothermic peak temperature (melting point Tmw2) of the second wax based on the DSC method and Tmw1 is expressed as 5+Tmw1 (&#xb0; C.)&#x2266;Tmw2 (&#xb0; C.)&#x2266;50+Tmw1 (&#xb0; C.).

Toner, process for producing toner, and two-component developing agent

Toner of the present invention includes aggregated particles formed by aggregating at least resin particles, pigment particles, and wax particles in an aqueous medium in the presence of a water-soluble inorganic salt. The wax includes at least one selected from the following: ester wax that has an iodine value of not more than 25, a saponification value of 30 to 300, and an endothermic peak temperature (melting point) of 50&#xb0; C. to 100&#xb0; C. based on a DSC method; and wax that is obtained by a reaction of alkyl alcohol having a carbon number of 4 to 30, unsaturated polycarboxylic acid or its anhydride, and synthetic hydrocarbon wax, and has an acid value of 1 to 80 mgKOH/g and an endothermic peak temperature (melted point) of 50&#xb0; C. to 120&#xb0; C. based on the DSC method. The toner and a two-component developer can achieve oilless fixing that prevents offset without using oil while maintaining high OHP transmittance, can eliminate spent of the toner components on a carrier to make the life longer, and can ensure high transfer efficiency by suppressing transfer voids or scattering during transfer.

Toner, method for producing toner, two-component developer, and image forming apparatus

Toner of the present invention is produced by mixing in an aqueous medium at least a resin particle dispersion in which resin particles are dispersed, a colorant particle dispersion in which colorant particles are dispersed, and a wax particle dispersion in which wax particles are dispersed and heating and aggregating the mixed dispersion. The main component of a surface-active agent used for the resin particle dispersion is a nonionic surface-active agent. The main component of at least one surface-active agent selected from a surface-active agent used for the wax particle dispersion and a surface-active agent used for the colorant particle dispersion is a nonionic surface-active agent. With this configuration, the toner can have a smaller particle size and a sharp particle size distribution without requiring a classification process. The toner and a two-component developer can achieve oilless fixing, eliminate spent of the toner components on a carrier to make the life longer, and ensure high transfer efficiency by suppressing transfer voids or scattering during transfer.

Toner, process for producing toner, two-component developer and image forming apparatus

Toner includes aggregated and associated particles formed by mixing in an aqueous medium at least a resin particle dispersion in which resin particles are dispersed, a colorant particle dispersion in which colorant particles are dispersed, and a wax particle dispersion in which wax particles are dispersed and heat-treating the mixed dispersion for aggregation. The aggregated and associated particles include first particles having a capsule structure in which aggregated wax with an average particle size of greater than 1 &#x3bc;m is incorporated into the resin, and second particles formed of the resin and the wax in a mixed and dispersed state. The toner can achieve oilless fixing that prevents offset without using oil while maintaining high OHP transmittance and also can eliminate spent of the toner components on a carrier to make the life longer.

Toner and two-component developer

The invention provides a method for preparing an ink having constituents of a water-soluble dye having a water-soluble solubilizing group of at least one of a sulfonic group and a carboxyl group, water, a water-soluble substance that is condensation-polymerized in the absence of the water, a water-soluble medium and an additive including at least one of an organic acid salt and an inorganic acid salt. This method includes a first mixing step of mixing at least the dye and the water-soluble substance out of the constituents of the ink excluding the additive; a second mixing step of mixing a mixture obtained in the first mixing step and the additive; and a pH adjusting step, performed before the second mixing step, of preparing a solution including the mixture or a solution including the additive while adjusting the solution to a given pH range by using a pH adjuster.

Method for preparing ink, ink cartridge and ink-jet recording apparatus

An ink-jet recording ink contains at least a colorant, a moisturizer, water and a water-soluble substance capable of undergoing polycondensation along with vaporization of the water, in which the colorant is a chelate azo dye.

Ink-jet recording ink, image forming method, ink-jet recording apparatus and imaged article

An ink composition is produced using a water-soluble substance that undergoes condensation polymerization in the absence of water (e.g., a hydrolyzable silane compound), which includes fluoroalkyl groups. Alternatively, a water-repellent film of a nozzle plate is subjected to a surface treatment with a trialkyl silane compound.

Ink composition for ink jet recording, ink cartridge, nozzle plate for ink jet recording, ink jet head, and recording apparatus

An aggregation stabilizer is further added to an ink composition for inkjet recording which contains a colorant, a humectant, water, and a water-soluble substance that is condensation-polymerized in the absence of the water. With this aggregation stabilizer, a hardly-soluble or insoluble component formed by the colorant and the water-soluble substance is modified so as to be readily dissolved in water, whereby generation of an aggregate in the ink is prevented.

Ink composition for inkjet recording, ink cartridge and recording apparatus

In ink containing a colorant, a humectant, a penetrant, water, and a water-soluble substance that is condensation-polymerized in the absence of the water (e.g., hydrolyzable silane compound), the surface tension of the ink at 25&#xb0; C. before the water-soluble substance is condensation-polymerized is set to 20&#x2013;50 mN/m, or the ink further contains a fluoroalkyl monoalcohol whose boiling point is lower than 100&#xb0; C.

Inkjet recording ink, solvent for use in said ink and cartridge and recording device having said ink

A filler solution of the present invention, which is supplied to fill an inkjet head, contains water and a hydrolyzate of a silicon compound which has a hydrophilic group.

Filler solution for inkjet head, inkjet head, and recording apparatus

Ink for ink-jet recording contains an oil soluble dye, a humectant, a penetrant, water, and an amphiphilic star block polymer of which the outer portion is hydrophilic. The surface tension of the ink at 25&#xb0; C. is in the range of 20 to 50 mN/m.

Ink for ink-jet recording, and ink cartridge and recording apparatus including the same

An ink composition containing a colorant, a humectant, water, and a water-soluble substance that begins to be condensation-polymerized as the water evaporates is ejected such that drops of the ink composition are adhered onto a print materialwhose surface is acidic, whereby an image is formed on the print material

Image formation method

In order to improve the water-resisting property of an image formed on a recording medium such as recording paper and plain paper by using an ink-jet recording ink, while also improving the light-resisting property of the image, an ink-jet recording ink, which contains a color material, water, a moisture-retaining agent, an organic silicon compound and an ultraviolet-ray absorbing agent, is allowed to contain an organic silicon compound in a range of 0.1 parts by weight to 50 parts by weight and an ultraviolet-ray absorbing agent in a range of 0.1 parts by weight to 10 parts by weight with respect to 100 parts by weight of the ink. The ultraviolet-ray absorbing agent is at least one compound selected from the group consisting of benzophenone-based, benzotriazole-based, cyanoacrylate-based and oxalic acid anilide-based compounds. Light energy of ultraviolet rays is converted to kinetic energy, heat energy and the like by the ultraviolet-ray absorbing agent at a predetermined concentration contained in the ink to prevent an amino group in the organic silicon compound from attacking an azo group in the color material due to the application of the ultraviolet rays. Alternatively, an ink-jet recording ink, which contains a color material, water, a moisture-retaining agent and an organic silicon compound, is arranged so that the organic silicon compound contains an ultraviolet-ray absorbing part, and the ultraviolet-ray absorbing part is prepared as at least one functional group selected from the group consisting of benzophenone-based, benzotriazole-based, cyanoacrylate-based and oxalic acid anilide-based functional groups. Alternatively, the ink is allowed to further contain an ultraviolet-ray absorbing agent having an acidic group.

Ink-jet recording ink, ink cartridge and recording device using such ink

A method of contacting a substrate having a surface containing hydroxyl groups with a non-aqueous solution containing a material having a chrolosilyl group; washing if desired; coating the substrate with a non-aqueous solvent containing a compound having a fluorocarbon group and a chlorosilane group or a solvent containing a compound containing a fluorocarbon group and an alkoxysilane; and baking the substrate if necessary in order to form a fluorocarbon-based polymer coating film chemically bonded to the substrate surface. The hydroxyl groups on the substrate surface and chlorosilyl groups are reacted to form a thin film having a large number of silanol groups (&#x2014;SiOH) capable of connecting the polymer coating film to the substrate to form a heat-, weather-, and wear-resistant film on various surfaces.

Method of manufacturing a fluorocarbon-based coating film

The present invention provides an ink composition for ink jet recording, including an azo dye, a humectant, water, and an amino-group-containing water-soluble compound that undergoes condensation polymerization in the absence of the water (e.g., an aminosilane compound), wherein a straight-chain or branched alkyl group whose carbon number is two or more, an alkoxyl group, a phenyl group or a derivative group thereof, a phenoxyl group, or a six-membered or larger cycloalkyl group is introduced to a carbon atom at an &#x3b1;-position of the amino group in the amino-group-containing water-soluble compound that undergoes condensation polymerization in the absence of water.

Ink composition for ink jet recording, ink cartridge containing the ink composition, and recording apparatus using the ink composition

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Osaka, Japan

Mamoru Soga