Mitsubishi Chemical Corporation

Mitsubishi Kasei Corporation

Nippon Steel Corporation

Mitsubishi Chemical Industries Limited

Nippon Pillar Packing Co., Ltd.

Mamoru Shoji

Tatsuo Ando

Hozumi Endo

Toshiaki Sasaki

Hisataka Hosoi

Hiroshi Maeda

Norio Ikeda

Takahisa Ueda

Terumasa Yamamoto

Masayuki Kasuya

Hitoshi Ohta

Masachika Yaguchi

Tatsuo Yamazaki

The present invention relates to a process for producing a laminated sheet comprising an alumina fiber precursor, which process comprises spinning out an alumina fiber precursor from a solution mainly comprising an aluminum compound, falling and stacking said alumina fiber precursor on the surface of an accumulator to form a thin lamina sheet of alumina fiber precursor, continuously pulling out said lamina sheet from the accumulator, transferring the resultant lamina sheet to a folding device, and folding the sheet by a predetermined width while stacking the folded sheet and continuously moving the stacking sheet in the direction orthogonal to the folding direction.

Process for producing laminated sheet comprising alumina fiber precursor

The heat-resisting material according to the present invention comprises a fiber aggregate containing crystalline alumina short fibers and formed in a continuous length and an inflammable sheathing for maintaining the shape of the fiber aggregate in a compressed state. The expansion percentage of the fiber aggregate after burn-off of the sheathing is not less than 10% by volume based on the volume of fiber aggregate in a compressed state. This heat-resisting material can be worked into various forms of product of the heat-resisting material such as rope, square bar, sheet, etc., according to the purpose of use. The present heat-resisting material is provided in continuously long products, has high heat resistance and restoring property, and can be easily applied to the openings or spaces ranged continuously in the longitudinal direction, such as the boundaries between the blocks of the heat-resisting material and joints.

Heat-resisting material

Monolith-holding element, process for producing the same, catalytic

A spinning nozzle for dry spinning a spinning solution containing a metal compound and an organic polymer compound by a blowing method. In the spinning nozzle, an air nozzle 6 is provided having a rectangular-prism-like slit which is formed by opposing inner surfaces, extending in parallel to each other. The opposing inner surfaces each include a projecting portion, which are formed at the front side of a pair of cover plates 1,1, with each of the projecting portions having a knife edge portion at its free end. Spinning solution supplying nozzles are composed of a plurality of linear pipes and are arranged in the air nozzle 6 in such a manner that they are in parallel to the parallel surfaces of the cover plates and project from the edges of the parallel surfaces. Air fed through a gas feeding port 5 and blown out as an air stream from the air nozzle 6, and streams of the spinning solution extruded from the spinning solution supplying nozzles form parallel streams. Further, the air stream in parallel to the spinning solution streams is sufficiently rectified so that it contacts the spinning solution. Accordingly, an amount of air used can be greatly reduced and fibers having excellent quality can be produced.

Process for preparing a fiber precursor of metal compound, and a process

A spinning nozzle for dry spinning a spinning solution containing a metal compound and an organic polymer compound by a blowing method. In the spinning nozzle, an air nozzle 6 is provided having a rectangular-prism-like slit which is formed by opposing inner surfaces, extending in parallel to each other. The opposing inner surfaces each include a projecting portion, which are formed at the front side of a pair of cover plates 1,1, with each of the projecting portions having a knife edge portion at its free end. Spinning solution supplying nozzles are composed of a plurality of linear pipes and are arranged in the air nozzle 6 in such a manner that they are in parallel to the parallel surfaces of the cover plates and project from the edges of the the parallel surfaces. Air fed through a gas feeding port 5 and blown out as an air stream from the air nozzle 6, and streams of the spinning solution extruded from the spinning solution supplying nozzles form parallel streams. Further, the air stream in parallel to the spinning solution streams is sufficiently rectified so that it contacts the spinning solution. Accordingly, an amount of air used can be greatly reduced and fibers having excellent quality can be produced.

Spinning nozzle for preparing a fiber precursor

An alumina fiber structure of a flat shape composed of alumina fibers having an alumina content of at least 65% by weight, the majority of said fibers being oriented substantially in parallel with the flat surfaces of the structure, and a number of fiber strands composed of the same alumina fibers extending inwardly from the flat surfaces of the structure, said structure having a thickness of from 4.8 mm to less than 10 mm, a density of from 0.07 to 0.3 g/cm.sup.3, a tensile strength of at least 0.5 kg/cm.sup.2 and a peeling strength of at least 0.5 kg/m.

Alumina fiber structure and process for its production

Alumina fiber structures prepared by (i) preparing precursor fibers by spinning a viscous spinning solution containing compounds of metals including aluminum and an organic polymer compound in which the proportion of alumina in the total metals in the solution is at least 65% by weight of alumina when all metals are calculated as their oxides; (ii) laying the precursor fibers into a mat; (iii) applying a lubricant which is a solution of higher fatty acid ester in a hydrocarbon solvent to the fibers either before or after forming the mat; (iv) needling the lubricated mat; and (v) burning the obtained structure to convert the precursor fibers to alumina fibers, possess high tensile strengths and high peel strengths.

An alumina fiber structure of a flat shape composed of alumina fibers having an alumina content of at least 65% by weight, the majority of said fibers being oriented substantially in parallel with the flat surfaces of the structure, and a number of fiber strands composed of the same alumina fibers extending inwardly from the flat surfaces of the structure, said structure having a thickness of at least 10 mm, a density of from 0.07 to 0.3 g/cm.sup.3, a tensile strength of at least 0.5 kg/cm.sup.2 and a peeling strength of at least 0.5 kg/m.

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Joetsu, Japan

Mamoru Shoji