The University of Arizona

Sandia Corporation

Battelle Memorial Institute

Duke University

Arizona Board of Regents, a Body Corporate

Thermo Jarrell Ash Corporation

Cid Technologies LLC

Spectro Analytical Instruments Gmbh & Co. Kg

M Bonner Denton

Roger P Sperline

Christopher A Gresham

Jeffrey Jon Zarnowski

Gary M Hieftje

Dong-Chul Pyun

Richard S Glass

Charles J Barinaga

Jason Amsden

David W Koppenaal

Eugene Atlas

Adi A Scheidemann

Dirk Ardelt

Joseph Carbone

Stephen W Czebiniak

Michael J Pilon

Steven N VanGorden

J Bruce True

Rafael Bento Serpa

Charles Parker

Scott Tilden

Elettra Piacentino

Justin Keogh

Rob Kingston

James H Barnes, Iv

Phillip J Rodacy

A virtual slit cycloidal mass spectrometer and spectrometry methods are disclosed. The spectrometer size-selects particles, which in turn serve as a 'virtual slit' for a cycloidal mass analyzer. This virtual slit provides unprecedented resolution in a system that takes up a much smaller physical footprint than was previously achievable. This spectrometer may facilitate field sampling of isotopes, such as uranium isotopes.

Virtual slit cycloidal mass spectrometer

Sulfur composites and polymeric materials having a high sulfur content and prepared from elemental sulfur as the primary chemical feedstock. The sulfur copolymers are prepared by the polymerization of elemental sulfur with one or more monomers of amines, thiols, sulfides, alkynylly unsaturated monomers, nitrones, aldehydes, ketones, thiiranes, ethylenically unsaturated monomers, or epoxides. The sulfur copolymers may be further dispersed with metal or ceramic composites or copolymerized with elemental carbon, photoactive organic chromophores, or reactive and solubilizing/biocompatible moieties. The sulfur composites and polymeric materials feature the ability self-healing through thermal reformation. Applications utilizing the sulfur composites and polymeric materials may include electrochemical cells, optics, HS donors and antimicrobial materials.

Sulfur composites and polymeric materials from elemental sulfur

An ion mobility spectrometer (IMS) for the detection of trace gaseous molecular compounds dissolved or suspended in a carrier gas, particularly in ambient air, without preconcentration or the trapping of analyte particles. The IMS of the invention comprises an ionization volume of greater than 5 cmand preferably greater than 100 cm. The larger size ionizers of this invention enable analysis of trace (&#x3c;1 ppb) of sample compounds in the gas phase. To facilitate efficient ion motion through the large volume ionization and reaction regions of the IMS, an electric field gradient can be provided in the ionization region or in both the ionization and reaction regions. The systems can be implemented with radioactive ionization sources, corona discharge ion sources or ions can be formed by photoionization. In specific embodiments, particularly when the sample gas is ambient air, the sample gas is heater prior to entry into the instrument, the instrument is run at temperatures above ambient, and the instrument can be heated by contact with heated sample gas exiting the instrument.

Sensitive ion detection device and method for analysis of compounds as vapors in gases

An apparatus for detecting particles, comprising a plurality of electrically conductive structures disposed on a support element. The structures are electrically insulated from one another and each structure can be electrically connected to an electronic read-out device. The structures receive a beam of particles in a direction forming an angle of incidence with the support element. A trough is disposed between each two successive structures as viewed in the beam direction. And at least partial overlap exists between each two successive structures. The apparatus can be disposed in the focal plane of a mass spectrometer.

Apparatus for detecting particles

A charged particle detector and method are disclosed providing for simultaneous detection and measurement of charged particles at one or more levels of particle flux in a measurement cycle. The detector provides multiple and independently selectable levels of integration and/or gain in a fully addressable readout manner.

Method and apparatus for simultaneous detection and measurement of charged particles at one or more levels of particle flux for analysis of same

A differential transimpedance amplifier circuit for correlated differential amplification. The amplifier circuit increase electronic signal-to-noise ratios in charge detection circuits designed for the detection of very small quantities of electrical charge and/or very weak electromagnetic waves. A differential, integrating capacitive transimpedance amplifier integrated circuit comprising capacitor feedback loops performs time-correlated subtraction of noise.

Differential transimpedance amplifier circuit for correlated differential amplification

An ion mobility spectrometer includes a drift tube having a collecting surface covering a collecting area at one end of the tube. The surface comprises a plurality of closely spaced conductive elements on a non-conductive substrate, each conductive element being electrically insulated from each other element. A plurality of capacitive transimpedance amplifiers (CTIA) adjacent the collecting surface are electrically connected to the plurality of elements, so charge from an ion striking an element is transferred to the capacitor of the connected CTIA. A controller counts the charge on the capacitors over a period of time.

Micro faraday-element array detector for ion mobility spectroscopy

Random access charge transfer devices are provided in which it is possible to simultaneously read electric charge that is stored within each detection element (pixel) that is in one of any desired combination of columns and that is also in one of any desired combination of rows. It is also possible to simultaneously read electric charge stored within each detection element or pixel in at least one selected column or row. In addition, it is possible to simultaneously cause injection of some or all of the electric charge stored in each detection element in one of any desired combination of columns and also in one of any desired combination of rows, or to simultaneously cause injection of some or all of the electric charge stored in each detection element in at least one selected column or row. In certain embodiments, a plurality of pre-amplifiers are connected to the column or row electrodes of the charge transfer device, for simultaneously producing a plurality of outputs, each output corresponding to the electric charge stored within at least one detection element or pixel in a single column or row, and a summation amplifier is provided having a feedback loop that is connected into each of the pre-amplifiers.

Collective charge reading and injection in random access charge transfer

A simultaneous multi-element atomic absorption spectrometry system includes a light source, a furnace, a spectrometer, and a random access charge transfer device. The furnace creates vapors of a sample contained within the furnace. The light source passes a light beam through the furnace so that wavelengths of the light beam corresponding to spectral lines of multiple elements contained in the vapors are absorbed by the vapors. The spectrometer receives the light beam after the light beam has passed through the furnace, and disperses the light beam into a spectrum. The random access charge transfer device receives the light beam after the light beam has passed through the spectrometer, integrates and stores charge corresponding to the intensity of the light beam, and randomly accesses for readout subarrays of the random access charge transfer device corresponding to spectral lines of the multiple elements. The spectrometry system also includes an optical apparatus that receives the light beam and shifts the light beam between a first and a second position.

Random access charge transfer devices for multi-element atomic

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Tucson, AZ, United States of America

M Bonner Denton