USA As Represented by Secretary of the Navy

Washington University

M Ashraf Imam

Virgil Provenzano

Teddy M Keller

Melvin H Miles

Arne W Fliflet

Bhakta B Rath

Donald U Gubser

Anand K Singh

Syed B Qadri

Edward P Gorzkowski, Iii

David Joseph Nagel

Satya B Sastri

William F Henshaw

Kuntimaddi Sadananda

Terry M Tritt

Norman P Louat

Nino R Pereira

Kuntimadi Sadananda

A multi-step method to produce materials, and coatings of materials, which has three key characteristics. The first is that the density of the resulting materials or coatings can be controllably and widely variable from less than ten percent of normal density up to normal density. The second key characteristic of the invention is the use of starting materials having powders that have grains (particles) with one, two or three dimensions on the size scales of nanometers or micrometers. The third major characteristic part of the invention is the use of microwave radiation or induction heating to quickly raise the temperature of the powders to produce materials or coatings before deleterious diffusion and densification can occur. These features produce new types of materials with properties favorable to many applications, such as chemical and other catalysis, electrolysis in batteries and fuel cells, and light weight structural components.

Sequential processing of materials and coatings of variable and controllable density with nanometer and micrometer sub-structures

This disclosure concerns a method of making silicon carbide involving adding agricultural husk material to a container, creating a vacuum or an inert atmosphere inside the container, applying conventional heating or microwave heating, heating rapidly, and reacting the material and forming silicon carbide (SiC).

Silicon carbide synthesis

A method of sintering by: placing a compacted metal powder inside a cylindrically-shaped susceptor and in an inert atmosphere or a vacuum, and applying microwave or millimeter-wave energy to the powder until the powder is sintered.

Sintering of metal and alloy powders by microwave/millimeter-wave heating

A composite material includes lithium hydride particles dispersed within lithium to form a lithium-lithium hydride composite. The lithium-lithium hydride composite has increased strength over pure lithium and similar soft X-ray transmission characteristics as pure lithium. A soft X-ray blast window may be made from the lithium-lithium hydride composite with increased reliability and cost effectiveness. A method for making a composite material includes dispersing lithium hydride into lithium metal using a variety of dispersion techniques.

Dispersion strengthened lithium and method therefor

Metal foams are impregnated with resins. The metal foam/polymer composite formed upon curing has excellent acoustic dampening and structural properties. Foams of various metals, such as aluminum, titanium, nickel, copper, iron, zinc, lead, silver, gold, platinum, tantalum, and alloys based on these metals, may be used. The polymer component may be any polymeric resin, for example, epoxy, natural rubber, acrylic, or phenolic.

Porous metal/organic polymeric composites

A palladium-boron composition and methods of making and using same are provided. In one aspect, the invention comprises an alloy comprising palladium and boron, the boron being in solid solution in the palladium and the alloy having a two-phase structure, wherein each phase of the two-phase structure has the same crystal structure as the other phase and has a different set of lattice parameters from the other phase such that the palladium is greatly hardened by the presence of the smaller phase crystals within the spaces between the larger phase crystals. The composition is carefully prepared by a process wherein palladium and an amount of boron sufficient to place the boron in solid solution, but insufficient to combine with the palladium, are placed together and repeatedly are melted, cooled and turned over until sufficiently mixed. The hardened composition can be used to create thinner membranes for hydrogen purification and improved electrodes for generation of heat energy, and other electrochemical processes.

Palladium-boron alloys and methods for making and using such alloys

A palladium-boron composition and methods of making and using same are provided. In one aspect, the invention comprises an alloy comprising palladium and boron, the boron being in solid solution in the palladium and the alloy having a two-phase structure, wherein each phase of the two-phase structure has the same crystal structure as the other phase and has a different set of lattice parameters from the other phase such that the palladium is greatly hardened by the presence of the smaller phase crystals within the spaces between the larger phase crystals. The composition is carefully prepared by a process wherein palladium and an amount of boron sufficient to place the boron in solid solution, but insufficient to combine with the palladium, are placed together and repeatedly arc melted, cooled and turned over until sufficiently mixed. The hardened composition can be used to create thinner membranes for hydrogen purification and improved electrodes for generation of heat energy, and other electrochemical processes.

A high temperature superconducting composite rod, wire or tape is formed by filling the open cells of a reticulated foam structure made of silver, silver alloy, gold or gold alloy with a superconducting ceramic oxide or precursor, compacting the filled structure and forming it into a rod, wire or tape and heating it to melt and/or texture the superconducting ceramic oxide. The resulting composite has continuous ligaments of metal throughout a continuous region of superconducting ceramic oxide.

High temperature superconducting ceramic oxide composite with reticulated metal foam

Method of making high temperature superconducting ceramic oxide composite with reticulated metal foam

Metal foams are impregnated with a phthalonitrile prepolymer. The metal f/polymer composite formed upon curing has excellent acoustic damping, structural properties, oxidative stability, and flame resistance. Foams of various metals, such as aluminum, titanium, nickel, copper, iron, zinc, lead, silver, gold, platinum, tantalum, and alloys based on these metals may be used.

Lightweight high damping porous metal/phthalonitrile composites

A metal composite material provides improved strength at all temperatures, in particular at those temperatures greater half the melting point of its matrix. The metal composite material is at least 50 volume percent hard particulate material in a matrix which is significantly more ductile than the hard particulate material. At or above 50 volume percent hard particulate material, each particle is surrounded by a thin film of the matrix material. This thin film resists deformation by converting sliding motion between particles into the rotational motion of the particles about each other. The matrix may be made by infiltrating a powder of the particulate material with a charge of the matrix material, for example, by hot isostatically pressing the matrix material into the powder or by melting a block of matrix material on top of the powder and thus infiltrating the powder by gravitational flow of the melted matrix material into the powder.

Superstrength metal composite material and process for making the same

Bulk form of superconducting materials are produced by pouring a melt a O.sub.2 -containing superconducting material into a heated mold, cooling the mold until solidification begins, removing the cast object from the mold, gradually cooling the cast object to prevent the development of thermal stresses, and then annealing the cast, cooled object to restore O.sub.2 to near equilibrium levels. The bulk form produced according to the present invention may be used as a sputtering target in the production of wires, or as a bulk form semiconductor.

Method of producing Bi-Sr-Ca-Cu-O superconducting materials in cast form

A high temperature superconducting coating of material oxide is produced by melting the metal oxide mixture, dipping a substrate, e.g. a platinum wire, in the metal oxide melt, withdrawing the substrate with a layer of metal oxide coated thereon, slowly cooling the metal oxide coating to avoid thermal shock and hot cracking, and post-annealing the metal oxide coating.

Growing community of inventors

Great Falls, VA, United States of America

M Ashraf Imam