Natural Fiber Welding, Inc.

Bradley University

United States of America, As Represented by the Secretary of Agriculture

Natural Fiber Wielding, Inc.

Luke Michael Haverhals

Aaron Kenneth Amstutz

Jonglak Choi

Spencer Jacob Null

Xiling Tang

Michael Molter

Skylar Clement

Isaiah Amstutz

Albert C Pierz

Ian T Pierz

Shang-Min Li

Zengshe Liu

Brent H Tisserat

Peter Francis Walker

Balmes Tejeda

Matthew Nelson

Nima Ezatollah Amini

Brent Baker

A thermoset material containing β-hydroxyesters wherein said thermoset material is subject to a mechano-chemical process to regenerate an epoxide and a carboxylic acid functionality. A curative for epoxidized plant-based oils and epoxidized natural rubber is created from the reaction between a naturally occurring polyfunctional acid and an epoxidized plant-based oil is disclosed. The curative may be used to produce porosity-free castable resins and vulcanize rubber formulations based on epoxidized natural rubber. Materials made from disclosed materials may be advantageously used as leather substitutes.

Curative and method

A welded yarn may have a cross section about a plane that is perpendicular to the longitudinal axis of the welded yarn wherein the cross-sectional area is comprised of two or more distinct portions, wherein the degree of welding in each portion is different, which May also result in different fiber volume ratios compared to raw yarn substrates.

Methods, processes, and apparatuses for producing welded substrates

An illustrative embodiment of a manufactured surface component may be comprised of a textile material on a first face and an elastomer material on a second face, wherein said elastomer material is bonded to said textile material, wherein said manufactured surface component is substantially planarly configured, wherein an area of said first face and said second face is from about 0.04 square inches to about 4.0 square inches, wherein a thickness of said manufactured surface component is from about 0.3 mm to about 2.5 mm, and wherein said manufactured surface component is substantially free of any petrochemical-derived plastics, petrochemicals, and toxins.

Curative

A curative for epoxidized plant-based oils and epoxidized natural rubber is created from the reaction between a naturally occurring polyfunctional acid and an epoxidized plant-based oil is disclosed. The curative may be used to produce porosity-free castable resins and vulcanize rubber formulations based on epoxidized natural rubber. Materials made from disclosed materials may be advantageously used as leather substitutes.

A curative for epoxidized plant-based oils and epoxidized natural rubber is created from the reaction between a naturally occurring polyfunctional acid and an epoxidized plant-based oil is disclosed. The curative may be used to produce at least one of six different materials, wherein each type of material may be configured as a thermosetting elastomer that is crosslinked with β-hydroxyester linkages. The materials may be configured as a leather-like material, a foam material, a molded elastomer, a coating, an adhesive, and/or a rigid or semi-rigid material. Illustrative articles made from any combination of the six materials may be recycled using a mechano-chemical process to de-crosslink the thermosetting elastomer.

A welding process may be configured to convert a substrate into a welded substrate by applying a process solvent to the substrate, wherein the process solvent interrupts one or more intermolecular force between one or more component in the substrate. The substrate may be configured as a natural fiber, such as cellulose, hemicelluloses, and silk. The process solvent may be configured as an ionic-liquid based solvent and the welded substrate may be a congealed network after the process solvent has been adequately swollen and/or mobilized the substrate. A welding process may be configured such that individual fibers of a substrate are not fully dissolved such that material in the fiber core may be left in the native state by controlling process variables. The welding process fibers may have a tenacity 10% or 20% greater or a diameter 25% less than that of a cellulosic-based yarn substrate.

Unique, inexpensive, and. strong biocomposites are obtained from blending cellulose matrix materials pith lignocellulosic reinforcement materials with the aid of alkaline aqueous solvent and cold temperatures. These lignocellulosic composites (LCs) are produced without use of any thermoplastic resins, adhesives, catalysts, plasticizers or d chemical or physical procedures. The LCs include a matrix and a reinforcement material. The matrix is a cellulose material (e.g., cotton, hemp, flax, or wood) that is liquefied using an aqueous alkaline solvent solution under cold temperatures to more readily adhere and or incorporate/encapsulate the lignocellulosic reinforcements (wood chips, fibers, and other lignocellulosic sources).

Lignocellulosic composites prepared with aqueous alkaline and urea solutions in cold temperatures systems

A dyeing and welding process may be configured to convert a substrate into a welded substrate having at least some color imparted thereto via a dye and/or coloring agent by applying a process solvent having a dye and/or coloring agent therein to the substrate, wherein the process solvent interrupts one or more intermolecular force between one or more component in the substrate. The substrate may be configured as a natural fiber, such as cellulose, hemicelluloses, and silk. The process solvent may include a binder, such as dissolved biopolymer (e.g., cellulose). After application of a process solvent comprised of a dye and/or coloring agent, the substrate may be exposed to a second application of a process solvent comprised of a binder, which second application may occur before or after a process temperature/pressure zone, process solvent recovery zone, and/or drying zone.

Methods, processes, and apparatuses for producing dyed and welded substrates

A coating created entirely from plant-derived ingredients is disclosed. Illustrative embodiments of the coating may be particularly well suited for use on leather-like materials created from epoxidized natural rubber-based formulations. Illustrative embodiments of the coating created may be comprised of substantially the reaction product between epoxidized vegetable oil and a polyfunctional naturally occurring acid (such as citric acid). Illustrative embodiments this reaction product may be used to produce porosity-free castable resins and vulcanize rubber formulations based on epoxidized natural rubber. Materials made from disclosed materials may be advantageously used as leather substitutes.

A thermoset material containing &#x3b2;-hydroxyesters wherein said thermoset material is subject to a mechano-chemical process to regenerate an epoxide and a carboxylic acid functionality. A curative for epoxidized plant-based oils and epoxidized natural rubber is created from the reaction between a naturally occurring polyfunctional acid and an epoxidized plant-based oil is disclosed. The curative may be used to produce porosity-free castable resins and vulcanize rubber formulations based on epoxidized natural rubber. Materials made from disclosed materials may be advantageously used as leather substitutes.

A curative for epoxidized plant-based oils and epoxidized natural rubber is created from the reaction between a naturally occurring polyfunctional acid and an epoxidized plant-based oil is disclosed. The curative may be used to produce at least one of six different materials, wherein each type of material may be configured as a thermosetting elastomer that is crosslinked with &#xdf;-hydroxyester linkages. The materials may be configured as a leather-like material, a foam material, a molded elastomer, a coating, an adhesive, and/or a rigid or semi-rigid material. Illustrative articles made from any combination of the six materials may be recycled using a mechano-chemical process to de-crosslink the thermosetting elastomer.

Growing community of inventors

Peoria, IL, United States of America

Luke Michael Haverhals