Learonal, Inc.

Luis H Garay

Donald W Thomson

Fred I Nobel

William R Brasch

Jason D Horowitz

Methods for the production of nickel or ammonium hypophosphite are disclosed, including combining sodium hypophosphite with nickel or ammonium sulfate to produce sodium sulfate and nickel or ammonium hypophosphite, and lowering the temperature of the solution containing the sodium sulfate to crystallize out the sodium sulfate.

Process for producing hypophosphite compounds

A method for preparing nickel hypophosphite by contacting a nickel anode with a solution of hypophosphite anions and applying a current through the anode to a counter-electrode in contact with the solution to anodically dissolve the nickel of the anode into the hypophosphite solution, thereby forming a nickel hypophosphite solution. A one-compartment electrolysis cell and a three-or-more-compartment electrodialysis cell embodying the method of the invention are described.

Nickel hypophosphite manufacture

Methods for preparing hypophosphorous acid are disclosed comprising contacting an insoluble anode with an aqueous solution of hypophosphite anions and applying a current through the insoluble anode to a cathode in electrical contact with the aqueous solution to generate H+ ions in the aqueous solution thereby forming a hypophosphorous acid solution.

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Rockville Centre, NY, United States of America

Luis H Garay