Research Institute of Petroleum Processing, Sinopec

China Petroleum & Chemical Corporation

China Petroleum Chemical Corporation

Lifeng Hu

Junyi Mao

Xiaojin Tang

Zhenxing Zhu

Shuandi Hou

Yongxiang Li

Zhihai Zhao

Zheng Liu

Tao Huang

Zhanzhu Zhang

Qing Yuan

Shaobing Wang

Hongliang Qu

Bo Zheng

Baoning Zong

Siyuan Qie

Zhiyong Pan

Guohua Gao

Jianqi Fei

A method for preparing 2-alkylanthracene includes the step of separating 2-alkylanthracene from a reaction product of anthracene alkylation reaction. The anthracene alkylation reaction is a reaction of anthracene and an alkylation reagent under an alkylation condition and in the presence of an alkylation reaction solvent and a catalyst. The reaction product of the anthracene alkylation reaction contains anthracene and the product of a series of alkylanthracenes containing 2-alkylanthracene.

Method for separating 2-alkylanthracenes and use thereof for producing hydrogen peroxide

The present disclosure generally relates to a liquid-solid radial moving bed reaction apparatus comprising a radial moving bed reactor, a spent catalyst receiver, a catalyst regenerator, and a regenerated catalyst receiver that are successively connected. Also disclosed is a solid acid alkylation process using the liquid-solid radial moving bed reaction apparatus.

Liquid-solid radial moving bed reaction device and solid acid alkylation method

A liquid-solid axial moving bed reaction and regeneration apparatus and a solid acid alkylation process by using the liquid-solid axial moving bed reaction and regeneration apparatus. the liquid-solid axial moving bed reaction and regeneration apparatus comprise: An axial moving bed reactor (), a spent catalyst receiver (), a catalyst regenerator () and a regenerated catalyst receiver () that are successively connected, wherein, a catalyst outlet of the regenerated catalyst receiver () is communicated with a catalyst inlet of the axial moving bed reactor (); Wherein, the axial moving bed reactor () is provided with at least two catalyst beds () arranged up and down, the axial moving bed reactor () is provided with a feed inlet () above each catalyst bed (); A catalyst delivery pipe () is arranged between two adjacent catalyst beds () so that the catalyst can move from top to bottom in the axial moving bed reactor (); A separation component () is provided between two adjacent catalyst beds (), the inside space of the separation component () is communicated with the catalyst delivery pipe (), the separation component () is for separating the stream after the reaction in the upstream catalyst bed from the catalyst, the catalyst obtained by the separation with the separation component () moves down through the catalyst delivery pipe ().

Liquid-solid axial moving bed reaction and regeneration device, and solid acid alkylation method

A liquid phase alkylation product from an alkylation reaction unit is introduced into a first heat-exchanger directly or after being pressurized with a pressure pump and heat-exchanged with a vapor phase stream from the column top of a high-pressure fractionating column n, then introduced into a second heat-exchanger and further heated to 100&#xb0; C.-150&#xb0; C., then introduced into the high-pressure fractionating column and subjected to fractionation at 2.0 MPa-4.0 MPa, the vapor phase stream from the column top of the high-pressure fractionating column is heat-exchanged with the liquid phase alkylation product to be separated, a liquid phase stream from the column bottom of the high-pressure fractionating column is introduced into a low-pressure fractionating column and subjected to fractionation under at 0.2 MPa-1.0 MPa, a low-carbon alkane is obtained from the column top of the low-pressure fractionating column n, and a liquid phase stream obtained from the column bottom of the low-pressure fractionating column is an alkylation oil product.

Process for separating alkylation product, alkylation reaction and separation process, and related apparatus

A process for separating an alkylation product includes introducing a liquid phase alkylation product from an alkylation reaction unit into a first heat-exchanger directly or after being pressurized with a pressure pump and heat-exchanged with a vapor phase stream from the column top of a high-pressure fractionating column, then into a second heat-exchanger and subsequently into the high-pressure fractionating column. The vapor phase stream from the column top of the high-pressure fractionating column is heat-exchanged with the liquid phase alkylation product to be separated, a liquid phase stream from the column bottom of the high-pressure fractionating column is introduced into a low-pressure fractionating column and subjected to fractionation under a condition of 0.2 MPa-1.0 MPa, a low-carbon alkane is obtained from the column top of the low-pressure fractionating column, and a liquid phase stream obtained from the column bottom of the low-pressure fractionating column is an alkylation oil product.

The present invention relates to a slurry bed loop reactor comprising a riser and at least one downcomer (), wherein two ends of the riser are connected to two ends of the downcomer () via lines () and (), respectively. The riser comprises a reaction section () and a settling section () with an increased tube diameter disposed on the reaction section (). A gas outlet () exists at the top of the settling section (). Each of the downcomers () is divided into a filtrate section () and a slurry section () by filter medium (), wherein the filtrate section () is connected to a liquid outlet (); two ends of the slurry section () are respectively connected to two ends of the riser, and the filtrate region () may further be connected to a back purging system. When used in a gas-liquid-solid three phases reaction system, the reactor can realize successive separation of gas, liquid and solid particles in slurry, and realize the back purging regeneration of filter tubes without influencing the reaction processes. In addition, said reactor has the advantages of high separation efficiency, simple structure, flexible and easy operation.

Slurry bed loop reactor and use thereof

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Beijing, China

Lifeng Hu