Shell Oil Comapny

Lawrence Walker Maas

Charles T Adams

Robert William Lewis

Richard A Geiman

A process is disclosed for removing color or color inducing impurities to petroleum derived wax by means of an adsorbent comprising a refined inorganic oxide having a pore distribution such that at least 60% of the pores possess a size of less than 350 Angstroms. Preferably, at least 90% of the pores possess a size of less than 350 Angstroms. The preferred inorganic oxide is an aluminum oxide and preferably has a surface area between 200 square meters per gram and 500 square meters per gram. A process is also disclosed for wax finishing utilizing multiple beds of refined alumina which may be operated in a swing bed fashion to intimately regenerate the refined alumina absorbent by such procedural steps as naphtha soaking, steam treating and heating in air.

Static bed wax decolorization process

A method for producing uninhibited transformer oil is disclosed which includes isolating a petroleum distillate that is primarily naphthenic and aromatic in character, boiling above 400.degree.F, having a viscosity between 50 and 100 SSU at 100.degree.F, and containing sulfur compounds; contacting the distillate with a solvent selective for aromatic hydrocarbons under conditions to produce a raffinate phase containing 15-30%v aromatic hydrocarbons; hydrotreating the raffinate phase to reduce the nitrogen content to at most 25 PPM, to maintain the sulfur content greater than 0.08%w, and to maintain the aromatic hydrocarbon content greater than 15%v. The product is an uninhibited transformer oil, and it can be further improved by regenerative clay treatment and by the addition of certain aromatic hydrocarbon compounds containing two or more six carbon membered fused or unfused rings, at least one of which is a benzene ring.

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Pasadena, TX, United States of America

Lawrence Walker Maas