Bodenseewerk Perkin-elmer Gmbh

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Bodenseewerk Perkin-elmer Co.

Klaus P Rogasch

Rolf G Tamm

Carl G Dencks

Gunther Roedel

Guenther Roedel

Device for generating a magnetic field in an atomic absorption

Method for analysis of samples by means of atomic absorption spectroscopy with electrothermal atomization of sample consists of the method steps: (a) introducing a liquid sample into a furnace, (b) heating the furnace up to a drying temperature for drying the sample, (c) subsequently heating the sample up to an atomizing temperature, in which a cloud of atoms develops in the furnace, in which cloud of atoms the components of the sample are present in atomic state, and (d) measurement of the atomic absorption of a measuring light beam with resonance spectral lines of an element looked for in the sample guided through the cloud of atoms. In this method (e), the vapors formed in the furnace during the heating of the furance up to the drying temperature are sucked off by a vacuum. Also, a device for carrying out this method is described.

Method and device for analyzing samples by means of atomic absorption

Atomic absorption spectrometer

A solenoid serves for generating a magnetic field at the location of a sample which is to be atomized in an atomic absorption spectrometer. A shift of the absorption lines of the atoms in a sample relatively to the emission lines in a measuring light beam (18) passed through the atomized sample is effected by the magnetic field due to the Zeeman effect. The solenoid (44) comprises a pair of pole pieces (46, 48) between which an air gap is formed. An atomizing device atomizes the sample within this air gap. Field coils generate a magnetic flux through the pole pieces (46, 48), the air gap and a magnetic return path (76). The field coils (60, 62) are arranged on pole pieces (46, 48) close to the air gap. The windings of the field coils (60, 62) are formed by tubes (216) which are designed to permit passage of a cooling liquid therethrough.

Electromagnet for an atomic absorption spectrometer

A burner assembly for an atomic absorption spectrometer having carrier (20) fixed to the burner head (14) and mounting a flame sensor (96) and an ignition device (16) so as to permit a single alignment of the flame sensor (18) and the ignition device (16) relative to the burner head (14) and subsequent movement or adjustment of the burner relative to the housing without changing the mutual positions of the ignition device (16) and the flame sensor (18) and while the flame is burning.

Burner assembly for atomic absorption spectrometer

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Uhldingen-Mulhofen, Germany

Klaus P Rogasch