Conoco Inc.

Keith M Roussel

John K Shigley

Ta-Wei Fu

Steve D Harris

Dave L Blakeburn, Ii

Robert R Griffin

Recarburizer coke containing not more than 0.1 weight percent sulfur and not more than 0.1 weight percent nitrogen is prepared by severe catalytic hydrotreating, followed by thermal cracking, and delayed coking of vacuum gas oil obtained from the vacuum distillation of FCC decant oil.

Process for the preparation of recarburizer coke

Premium coke having a low coefficient of thermal expansion and containing reduced fluff coke is obtained by subjecting an aromatic mineral oil to reduced temperature delayed coking, thereafter converting uncoked oil in the coke drum to coke under delayed coking conditions by continuing coking in the presence of a aromatic mineral oil capable forming coke admixed with a non-coking material circulated through the coke drum as a heating fluid. After termination of the heating fluid, the coke in the coke drum is subjected to a heat soak in the presence of a non-coking material at an elevated temperature preferably above the delayed coking conditions.

Delayed coking process

The present invention resides in improved graphite nipples which are suitable for connecting graphite electrodes. The graphite nipples are prepared by adding mesophase pitch-based carbon fibers into a typical nipple extrusion blend.

Method of making graphite electrode nipple

Binder pitch is prepared by combining a petroleum aromatic mineral oil thermal tar and super finely subdivided calcined premium coke particles. The petroleum aromatic mineral oil thermal tar is obtained by hydrotreating, thermally cracking and vacuum distilling an aromatic mineral oil. Additionally, the aromatic mineral oil thermal tar may be subjected to heat soaking.

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Ponca City, OK, United States of America

Keith M Roussel