Agency of Industrial Science and Technology

Ministry of International Trade & Industry

Aisin Seiki Kabushiki Kaisha

National Industrial Research Institute of Nagoya

Agency of Industrial Science and Technology Ministry of International

Kazutaka Suzuki

Shoichi Kume

Haruo Yoshida

Michihide Machida

Yasuhiro Enya

Yoshinori Nishida

Akinari Ishikawa

Yoshio Tasaki

Shiro Ikuta

Takashi Sakurai

Masamitu Ishikawa

Haruo Yoshido

The purpose of the present invention is to provide a titanium nitride aluminum based sintered material having excellent durability and able to be cheaply produced and cut spheroidal graphite cast iron at high speed and be used as a cutting tool material having a long life, and a method of production the same. The present invention resides in a production method of a titanium nitride aluminum based sintered material characterized in that powder of Ti.sub.(1-x) Al.sub.x N (x=0.05.about.0.70) is sintered. Said x is preferably set to a range from 0.05 to 0.15 or from 0.50 to 0.70. 0.2 to 11.1% of an additive by volume constructed by TiO.sub.y (y=1.about.2) and/or Al.sub.2 O.sub.3 is preferably externally added to the above titanium nitride aluminum based sintered material.

Titanium nitride aluminum based sintered material and its production

The purpose of the present invention is to provide a cubic boron nitride based sintered material having excellent durability and capable of cutting at least spheroidal graphite cast iron at high speed and usable in a cutting tool having a long life, and a production method of this cubic boron nitride based sintered material. The present invention resides in a production method of a cubic boron nitride based sintered material characterized in that a mixing raw material is produced by mixing powder of Ti.sub.(1-x) Al.sub.x N(x=0.05.about.0.70) and the powder of a cubic boron nitride, and is next sintered. A compounding ratio of the above mixing raw material is preferably set such that this mixing raw material includes 10 to 90% of the above Ti.sub.(1-x) Al.sub.x N(x=0.05.about.0.70) by volume and 10 to 90% of the above cubic boron nitride by volume.

Cubic boron nitride based sintered material and its producing method

A cubic boron nitride-containing high-density inorganic composite is prepared by mixing cubic boron nitride with a powdered inorganic compound capable of forming a rigid sintered article having a density of at least 85% and a Vickers hardness of at least 800, which does not promote the conversion of cubic boron nitride into graphite-type phase boron nitride (hBN). The powder mixture is compressed into a mold, and fired at low pressure of between 1,000-2,000 MPa, at a temperature of not more than 1,500.degree. C., under which conditions the cubic boron nitride does not convert to hBN, but is sufficiently metastable to permit the formation of the high-density inorganic composite.

Method for production of cubic boron nitride-containing high-density

A cubic boron nitride-containing high-density inorganic composite sintered article is produced by a method which essentially consists of preparing a mixture of a cubic boron nitride powder with an inorganic compound powder capable of forming a high-rigidity sintered article under the conditions permitting the cubic boron nitride to remain in a substantially metastable, though not thermodynamically stable, state, a mixture of an inorganic compound-coated cubic boron nitride powder with an inorganic compound powder, or an inorganic compound-coated cubic boron nitride powder, and sintering the mixture of the cubic boron nitride powder with an inorganic compound powder, the mixture of the inorganic compound-coated cubic boron nitride powder with an inorganic compound powder or an inorganic compound-coated cubic boron nitrides powder, under the conditions of not more than 2,000 MPa of pressure and not more than 1,500.degree. C. of temperature for permitting the cubic boron nitride to remain in a substantially metastable, though not thermodynamically stable, state for a period incapable of causing conversion of the cBN into a graphite-type phase.

Method of production of cubic boron nitride-containing high-density

A sintered article of diamond is obtained by coating the surface of diamond particles with 30 to 0.1% by volume, based on the total volume of the diamond particles and aids, of at least one member selected from the group consisting of the transition metals of Groups 4a, 5a, and 6a in the Periodic Table of Elements and boron and silicon, and sintering the coated diamond particles under conditions of high pressure and high temperature, which sintered article consists of 70 to 99.8% by volume of diamond and 30 to 0.2% by volume of the carbide of the coating substance. A method for the production of the sintered article of diamond is also disclosed.

Sintered article of diamond and method for production thereof

Method for production of a sintered article of diamond

Growing community of inventors

Nagoya, Japan

Kazutaka Suzuki