Stora Enso Oyj

Katja Lyytikäinen

Isto Heiskanen

Kaj Backfolk

Esa Saukkonen

Jukka Kankkunen

Anna Kauppi

Ville Ribu

Heidi Saxell

Nina Ruohoniemi

Otto Nylén

Juha Korvenniemi

The present invention relates to a method for manufacturing a multilayer film comprising microfibrillated cellulose (MFC) in a paper-making machine, the method comprising the steps of: a) forming a bottom web layer by applying a first pulp suspension comprising at least 50% by dry weight of cellulose based fibrous material having an SR (Schopper-Riegler) value in the range of 18-75 on a bottom web wire; b) forming or applying an intermediate web layer formed from a second pulp suspension comprising at least 50% by dry weight of MFC having an SR value in the range of 80-100 on the bottom web layer; c) applying a top web layer formed from a third pulp suspension comprising at least 50% by dry weight of cellulose based fibrous material having an SR (Schopper-Riegler) value in the range of 18-75 on the intermediate web layer to form a multilayer web; and d) dewatering, and optionally drying, the formed multilayer web to obtain a multilayer film comprising MFC.

Multilayer film comprising MFC

The present invention relates to a method for the production of an adhesive component wherein said method comprises the following steps: providing a suspension comprising starch granules, adding a suspension comprising microfibrillated cellulose to the suspension comprising starch granules, drying the starch granules and microfibrillated cellulose suspension to a dry content above 70 wt-% to form said adhesive component. The invention also relates to an adhesive, a corrugated board, paper and paperboard comprising said adhesive and to the adhesive component produced according to the method.

Method to produce an adhesive component comprising starch and microfibrillated cellulose, an adhesive and products

The present invention is directed to a coated paper substrate that is particularly suitable for metallization and other nano-coatings that provide barrier properties and are applied using vacuum deposition techniques. The invention is also directed to a process for preparing the coated paper substrate. The invention is also directed to a packaging material comprising the coated paper substrate.

Coated paper substrate suitable for metallization

The present invention relates to a method for manufacturing a multilayer film comprising highly refined cellulose fibers, the method comprising the steps of: a) forming a first wet web by applying a first pulp suspension comprising highly refined cellulose fibers on a first wire; b) partially dewatering the first wet web to obtain a first partially dewatered web; c) forming a second wet web by applying a foamed second pulp suspension comprising highly refined cellulose fibers and a foaming agent on a second wire; d) partially dewatering the foamed second wet web to obtain a second partially dewatered web; e) joining the first and second partially dewatered web to obtain a multilayer web; and f) further dewatering, and optionally drying, the multilayer web to obtain a multilayer film comprising highly refined cellulose fibers.

Multilayer film comprising highly refined cellulose fibers

The present invention relates to a method for manufacturing a multilayer film comprising highly refined cellulose fibers, the method comprising the steps of: a) forming a first wet web by applying a first pulp suspension comprising highly refined cellulose fibers on a first wire; b) partially dewatering the first wet web to obtain a first partially dewatered web; c) forming a second wet web by applying a second pulp suspension comprising highly refined cellulose fibers on a second wire; d) partially dewatering the second wet web to obtain a second partially dewatered web; e) applying a binder between the first and second partially dewatered web and joining the first and second partially dewatered web to obtain a multilayer web; and f) further dewatering, and optionally drying, the multilayer web to obtain a multilayer film comprising highly refined cellulose fibers.

The present invention relates to a method for preparing a surface-treated fibrous material comprising nanocellulose, in which a fibrous material is surface treated with an organic acid or salt thereof. Fibrous materials as such are also provided. The present technology allows improved Water Vapor Transmission Rates (WVTR) for the fibrous material, while operating on an industrial scale.

Method for treating a fibrous material comprising nanocellulose with an organic acid or organic acid salt

The present invention relates to a method for manufacturing a film comprising microfibrillated cellulose wherein the method comprises the steps of; providing a suspension comprising a microfibrillated cellulose, adding an enzyme to the suspension, mixing the enzyme with the suspension to form a mixture, applying said mixture to a wire to form a fibrous web and drying said web to form said film. The present invention further relates to a film comprising microfibrillated cellulose having good barrier properties.

Method for producing a film having good barrier properties and a film having good barrier properties

A method of manufacturing a film having an oxygen transmission rate (OTR) value in the range of 0.1 to 200 cc/m*24 h at 23&#xb0; C., 50% relative humidity (RH), and an OTR value in the range of 0.1 to 2000 cc/m*24 h at 38&#xb0; C. at 85% RH, comprising at least 60% by weight nanocellulose based on the weight of the total amount of fibers in the film, wherein the method comprises the steps of, providing an aqueous suspension comprising said nanocellulose; forming a web from said aqueous suspension; calendering said web at a line load of at least 40 kN/m, and at a temperature of at least 60&#xb0; C. wherein said film is formed and said web has an OTR value in the range of 50 to 10 000 cc/m*24 h at 23&#xb0; C., 50% RH before said calendering step, or more preferably in the range of 500 to 5000 cc/m*24 h at 23&#xb0; C., 50% RH before said calendering step.

Method of manufacturing a film having low oxygen transmission rate values

The present invention relates to a method for manufacturing an intermediate product that can be stored and transported and efficiently converted into microfibrillated cellulose with limited energy input at the time of conversion. More specifically, the invention involves the use of dewatered carboxymethylcellulose or carboxylated cellulose fiber having a low degree of substitution and a high amount of additives.

Method for manufacturing intermediate product for conversion into microfibrillated cellulose

Method for making a film that comprises microfibrillated cellulose, wherein the film has low OTR values and especially suitable for a tropical environment. The method comprising the steps of providing a suspension comprising microfibrillated cellulose (MFC), forming a film from said suspension, wherein the film having a solid content above 40%, preferably above 50%, treating the film with flame or plasma treatment, such that a surface activation takes place on the film, and cooling the film, wherein the surface of the film having a decreased OTR value and a high moisture resistance.

Method for making a film comprising MFC

A method for the production of a fibrous product from a fibrous web, wherein the method comprises the steps of: &#x2014;providing a fibrous suspension comprising a microfibrillated cellulose, wherein the content of the microfibrillated cellulose of said suspension is in the range of 60 to 99.9 weight-% based on total dry solid content, &#x2014;adding an uncharged, amphoteric or weakly cationic polymer having a molecular weight of at least 50000 g/mol to said suspension, &#x2014;adding an anionic polymer having a molecular weight of at least 00000 g/mol to said suspension to provide a mixture of said microfibrillated cellulose, said uncharged, amphoteric or weakly cationic polymer and said anionic polymer, 1&#x2014;providing said mixture to a substrate to form a fibrous web, wherein the amount of uncharged, amphoteric or weakly cationic polymer in said mixture is in the range of 0.1 to 20 kg/metric ton based on total dry solid content and wherein the amount of anionic polymer in said mixture is in the range of 0.01 to 10 kg/metric ton based on total dry 20 solid content; and&#x2014;dewatering said fibrous web to form a fibrous product.

Method to produce a fibrous product comprising microfibrillated cellulose

The present invention relates to a new process for improving dewatering when manufacturing a film comprising high amounts of microfibrillated cellulose (MFC) without negatively impacting the film properties. According to the present invention a high amount of nanoparticles is used as an additive, optionally together with a polymer.

Process for production of film comprising microfibrillated cellulose

The present invention relates to an UV blocking film comprising microfibrillated cellulose wherein at least part of the microfibrillated cellulose is microfibrillated cellulose produced from non-chemical modified lignocellulosic material. The invention also relates to a method for producing the film, use of said film as well as a composition having UV blocking properties.

UV blocking film and composition comprising microfibrillated cellulose, a method for producing said film and use of the composition

The present invention relates to a method for manufacturing a film having an oxygen transmission rate in the range of from 1 cc/m/24 h to 500 cc/m/24 h according to ASTM D-3985, at a relative humidity of more than 50% at 25&#xb0; C., or higher than 75% at 25&#xb0; C., or higher than 85% at 25&#xb0; C., wherein the method comprises the steps of: providing a first suspension comprising a microfibrillated cellulose, wherein the dry content of the suspension is in the range of from 0.1 to 10% by weight, adding a wet strength additive to said first suspension, at an amount of from 0.1 to 10 weight-% based on the amount of microfibrillated cellulose (dry/dry), thereby forming a mixture of the microfibrillated cellulose and the wet strength additive, applying said mixture to a substrate to form a fibrous web and drying said web to form said film. The present invention also relates to a film produced according to the method.

Method for producing a film having good barrier properties

A method of manufacturing a film comprising microfibrillated cellulose, wherein the method comprises the steps of: providing a first suspension comprising microfibrillated cellulose, having a dry content of from 0.2 to 2.0%, wherein the first suspension has a first Schopper-Riegler (SR) value; forming a first web of said suspension; at least partly dewatering said first web; applying a second suspension comprising microfibrillated cellulose, and/or fines and/or fibers onto a surface of said formed and at least partially dried first web, wherein the second suspension has a second Schopper-Riegler value which is higher than said first Schopper-Riegler value, thereby forming a film.

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Imatra, Finland

Katja Lyytikäinen