Zhejiang Juhua Co.,ltd.electrochemistry Plant

Zhejiang Quzhou Jusu Chemical Industry Co.,ltd

Junming Lu

Zhigang Wu

Xinben Zhao

Lanhui Su

Yupeng Wu

Congli Ma

Jinming Han

Gang Su

Yudeng Chai

Hongxin Zhou

Disclosed are a heat-expandable polyvinylidene chloride microsphere and its preparation method. The preparation method comprises: by weight, dissolving 250 to 550 parts of an aqueous-phase polymerization inhibitor, 20 to 100 parts of a dispersant, and 3 to 15 parts of a co-dispersing monomer in deionized water, adjusting a pH value of the solution and cooling the solution to obtain an aqueous phase for later use; dissolving 5 to 15 parts of a cross-linking agent and 20 to 45 parts of an initiator in 1000 to 2000 parts of a mixed monomer, and cooling the solution to obtain an oil phase for later use; mixing and homogenizing the aqueous phase and the oil phase with stirring to obtain a homogenized mixed solution; adding 300 to 550 parts of a foaming agent to the homogenized mixed solution and homogenizing the resulting solution with stirring to obtain a homogenized mixed solution containing the foaming agent; reacting the homogenized mixed solution containing the foaming agent with stirring; at the end of the reaction, cooling to room temperature, filtering the resulting suspension to obtain filtrate, centrifuging and dehydrating the filtrate, and drying to obtain the heat-expandable polyvinylidene chloride microsphere product. This disclosure has the advantages of simple process and environmental friendliness, and the obtained product has good performance.

Heat-expandable polyvinylidene chloride microsphere and its preparation method

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Zhejiang, China

Junming Lu