Shimadzu Corporation

Shimadzu Seisakusho Ltd.

Junichi Ono

Isao Fukui

Naoki Imamura

A method of emission spectrochemical analysis is provided which comprises the steps of producing a predetermined number of spark discharges between an electrode and a specimen containing an element in a first and second state. The intensity of emission of light caused by each of the spark discharges is measured and a frequency distribution of the measured intensities of emission is obtained. The distribution is separated into an area of normal distribution and an area outside the area of normal distribution, and an intensity of emission value is selected. The amount of the element in the first state is determined as a function of the selected intensity of emission multiplied by the area of normal distribution and the amount of the element in the second state is determined as a function of the selected intensity of emission multiplied by the area outside the area of normal distribution.

Method for emission spectrochemical analysis

Apparatus for emission spectrochemical analysis wherein the sample to be analyzed is excited by repeated spark discharge to emit light, which is dispersed to produce a spectrum containing emission lines characteristic of the elements in the sample. The intensity or quantity of light of each of the emission lines of the elements to be determined and that of the corresponding one of the emission lines selected as the internal standards for the elements to be determined are measured each time a spark discharge is produced to obtain the ratio of the former intensity or quantity to the latter at each spark discharge, and the ratios resulting from a predetermined number of spark discharges are averaged for each of the elements to be determined. From the average the content of each of the elements is read on a calibration curve.

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Kyoto, Japan

Junichi Ono