Rohm and Haas Company

Air Products and Chemicals, Inc.

Rohn and Haas Company

John Hiroshi Yamamoto

Won Suh Park

Stephen Gerard Maroldo

Sergei Vladimirovich Ivanov

Curtis Alan Schwartz

Randall Wayne Stephens

Arthur A Chin

Rajiv Monohar Banavali

Michael M Cook

Francis Lipiecki

Aaron Sarafinas

Anthony Rocco Cartolano

Samuel J November

Puja Jain

Cheryl Irene Teich

Suzanne Linehan

Rajiv Manohar Banavali

Arthur Achhing Chin

Francis Joseph Lipiecki

A process for production of a borohydride compound. The process comprises combining a compound comprising boron and oxygen with an adduct of alane.

Process for production of a borohydride compound

A method for preparing an amine borane from an alkali metal borohydride and an amine salt. The alkali metal borohydride is allowed to react with 0.95 to 1.05 equivalents of the amine salt in a solvent which contains water and an amine.

Synthesis of amine boranes

A stabilized aqueous mixture containing at least one borohydride compound and at least one metal hydroxide compound. The mixture has improved stability with regard to decomposition of borohydride, especially at elevated temperatures.

Stable high-temperature borohydride formulation

A method for producing MBH, wherein M is a metal or ammonium cation and n is one or two, by combining a metal borohydride and XBH; wherein X is a substituted amine; a substituted phosphine; or tetrahydrofuran.

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The present invention relates to a method of making lithium borohydride that gives high yields while maintaining ease of purification.

Method of making lithium borohydride

A method for preparing a lithium aluminum hydride solution comprising lithium aluminum hydride, toluene and tetrahydrofuran by the steps of: (a) combining lithium chloride, tetrahydrofuran, and a slurry of sodium aluminum hydride in toluene; and (b) allowing the mixture formed in step (a) to react to form a product mixture comprising lithium aluminum hydride, sodium chloride, tetrahydrofuran and toluene.

Method for preparation of lithium aluminum hydride from sodium aluminum hydride

A method for reducing a malonate having the formula R R C(CO R )(CO R ) to a diol having the formula R R C(CH OH) comprising treating said malonate with sodium aluminum hydride.

Method for reduction of substituted malonates to diols

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New Britain, PA, United States of America

John Hiroshi Yamamoto