Rheometrics, Inc.

John F Blanch

William David Richards

Joseph C Golba, Jr

Ronald F Garritano

On-line rheological measurements are made utilizing a rheometer of the type in which a first metering pump delivers diverted melt from a process main stream to a capillary passage and a second metering pump returns the diverted melt from the capillary passage to the process main stream and the viscosity of the diverted melt is measured by controlling the rate of flow of the melt to maintain constant the pressure drop between spaced apart locations along the capillary passage and measuring the temperature of the melt in the capillary passage. The measurements may be made while controlling the speed of the second metering pump independent of the speed of the first metering pump to maintain the pressure at the exit of the capillary passage essentially constant. The capillary passage is placed in close proximity to the process main stream for maintaining a relatively short residence time during which the diverted melt resides outside the process main stream so as to attain a relatively quick response to changes in the measured viscosity. The rheometer includes a relatively thin plate interposed between first and second blocks, the plate including a slot establishing a chamber between the first and second blocks for providing the capillary passage.

On-line rheological measurements

A test fixture for use in measuring the forces required to bend a test specimen throughout a range of temperatures includes clamps for gripping the ends of the test specimen while bending forces are applied intermediate the ends of the specimen, the clamps being carried by carriages movable in directions aligned with the test specimen and biased away from one another by constant force springs so that movement of the ends of the test specimen is permitted in response to temperature changes in the test specimen, against the constant bias of the constant force springs, thereby maintaining the test specimen in constant tension during the measurement of bending forces despite the changes in temperature.

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Mantoloking, NJ, United States of America

John F Blanch