Basf Se Corporation

Joachim Wulff-Doering

Johann-Peter Melder

Manfred Julius

Rainer Papp

Frank-Friedrich Pape

Frank Haese

Ulrich Koehler

Gunter Lipowsky

Peter Zurowski

Mirko Haider

Peter Gaa

Juergen Strasser

Kathrin Luise Mariethres Werth

A process for preparing oligo ethylene glycol methyl ether borate involves feeding boric acid and oligo ethylene glycol monomethyl ether into a reactor, and reacting to obtain a raw product containing oligo ethylene glycol methyl ether borate, water, and unreacted boric acid and oligo ethylene glycol monomethyl ether. The raw product is fed to a reactive distillation device and boric acid is reacted with oligo ethylene glycmonomethyl ether for full conversion of boric acid. A distillate stream containing water is transferred from the top of the reactive distillation device to a condenser, and a condensed liquid stream is recycled to the top of the reactive distillation device. A bottom product stream containing oligo ethylene glycol methyl ether borate is withdrawn from the reactive distillation device. The bottom product stream is partially recycled to a reboiler. The resulting vapor stream is recycled to the bottom of the reactive distillation device.

Process for preparing oligo ethylene glycol methyl ether borate

Processes comprising: providing an aromatic alcohol; and reacting the aromatic alcohol with ammonia at a temperature of 80 to 350&#xb0; C. in the presence of hydrogen and a heterogeneous catalyst to form a crude reaction product comprising a corresponding primary aromatic amine, wherein the heterogeneous catalyst comprises a catalytically active composition which, prior to reduction with hydrogen, comprises 90 to 99.8% by weight of zirconium dioxide (ZrO), 0.1 to 5.0% by weight of an oxygen-comprising compound of palladium, and 0.1 to 5.0% by weight of an oxygen-comprising compound of platinum.

Method for the continuous production of an amine

The present invention relates to a process for preparing tertiary alkyl esters of (meth)acrylic acid having at least 4 carbon atoms in the alkyl radical. The process includes reacting (meth)acrylic acid with at least one olefin of formula (I) in homogeneous phase in the presence of an acidic catalyst in a reactor, discharging the resulting reaction mixture from the reactor, separating the discharged reaction mixture into a first mixture which contains the catalyst and a second mixture which contains the tertiary alkyl ester of (meth)acrylic acid having at least 4 carbon atoms in the alkyl radical, and removing the tertiary alkyl ester of (meth)acrylic acid having at least 4 carbon atoms in the alkyl radical from the second mixture in the presence of compound S, which comprises at least one N-oxyl group and is added as a stabilizer.

Process for preparing tertiary alkyl esters of (meth)acrylic acid having at least 4 carbon atoms in the alkyl radical

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Frankenthal, Germany

Joachim Wulff-Doering