Southwest Petroleum University

Chengdu Leps Technology Co., Ltd

Uti Limited Partnership

Chengdu University of Technology

Jianchun Guo

Chi Chen

Bo Gou

Cong Lu

Shan Ren

Xiao Li

Shaobin Zhang

Jichuan Ren

Bin Liu

Kun Wang

Zhihong Zhao

Su Diao

Qingsong Guo

Qianli Lu

Yong Ren

Congbin Yin

Chao Liu

Tao Zhang

Yuxuan Liu

Meiping Li

Ye Zhong

Jie Lai

Chaojun Tang

Yang Lu

Jiapeng Zhang

Mingyong Zeng

Mingyuan Zhou

Zhuang Liu

Hangyu Zhou

Yunchuan Zheng

Tao N Zhang

Haiyan Zhu

Tao Liu

Bo Yang

Gang Li

Xianjun He

Yuanhua Lin

Hao Yang

Yapu Zhao

Shouxin Wang

Li Ma

Le He

Ming Li

Xuanhe Tang

Zhi Wang

Chuhao Huang

Yongchun Zhang

Fenglan Huang

Binwei Xu

Zishuo Li

Yangang Jiang

Shenyan Gou

Xiaohong Wang

Songgen He

Jiyu Wang

Feng Zhao

Yingxian Ma

Liang Tao

Xin Lei

Mingzhong Chen

Pengcheng Tang

Li Zhan

Xinghao Gou

Guangyao Yang

Bin Qian

Xueshan Yang

Ji Zeng

Junyao Ran

Hao Ou

Yangyi Xing

Shilei Xu

Hengbo Zuo

Yongxin Zhu

Yongjun Xiao

Xiangzeng Wang

Shibin Wang

Youjing Duan

Jiandong Wang

Shiyan Hao

Dilin Wen

Fanhui Zeng

Peng Shi

Ruimin Gao

Zhangxing Chen

Xiang Bai

Yang Luo

Huifei Mao

Xinfeng Jia

Feng Shen

Xiaozhao Cheng

Hongmei Wang

Fuhu Chen

Nianxi Wang

Jamie Mcinnis

Shouyi Wang

Jinqiao Wu

Kun Sun

Jun Ni

Junfeng Li

Yu Zhang

A suspended sand dragging fiber and a preparation method thereof, the method including: dispersing nanoparticles into a first solvent, adding a coating agent and a flexibilizer to the first solvent, and stirring and aging to obtain a surface treatment agent; adding a surfactant to a second solvent, adding alkyl polyether siloxane to the second solvent after the surfactant is dissolved in the second solvent, and stirring to obtain a finishing agent; transferring the surface treatment agent to a sizing trough of a sizing machine, sizing polyester fibers using the sizing machine, and drying and curing to obtain surface-modified fibers, and diluting the finishing agent to obtain a finishing agent solution, and treating the surface-modified fibers with the finishing agent solution to obtain the suspended sand dragging fiber.

Suspended sand dragging fibers and preparation methods thereof

The present disclosure provides a high-temperature-resistant deep penetration molecular membrane acid copolymer and a preparation method thereof. The copolymer is formed by polymerizing four raw monomers including 2-acrylamido-2-methylpropanesulphonic acid, vinyl phosphonic acid, alkyl dimethylallyl ammonium chloride, and perfluoropolyether acrylate. The method comprises: S1: mixing and stirring solvent oil, an emulsifier, the alkyl dimethyl allyl ammonium chloride, and the perfluoropolyether acrylate to be dispersed homogeneously to obtain an oil phase; S2: mixing and stirring the 2-acrylamido-2-methylpropanesulphonic acid, the vinyl phosphonic acid, a complexing agent, and distilled water, and adjusting pH to obtain an aqueous phase; S3: slowly dropwise adding the aqueous phase to the oil phase; and S4: introducing nitrogen into the water-in-oil emulsion to remove oxygen, then adding an initiator and carrying out a heating polymerization reaction to obtain copolymer emulsion (i.e., a molecular membrane agent). The copolymer emulsion is added to an acid solution to obtain molecular membrane acid.

High-temperature-resistant deep penetration molecular membrane acid copolymers and preparation methods thereof

The present invention pertains to the field of oilfield stimulation technologies for oil and gas field development, in particular to an instant soluble temperature and salt resistant polyacrylamide and the preparation method and application thereof, and the polyacrylamide is modified by adding rigid temperature and salt resistant monomer containing benzene ring and cationic fluorinated hydrophobic monomer on the basis of acrylamide monomer and sodium acrylate monomer, and then polymerized to obtain instant soluble temperature and salt resistant polyacrylamide. The temperature and salt resistant monomer containing benzene ring can improve the thermal stability and temperature and salt resistance of polyacrylamide, while the long-chain cationic fluorinated hydrophobic monomer can enhance the hydrophobicity of polymer. The comprehensive properties of polymer is improved by appropriate intermolecular association.

Instant soluble temperature and salt resistant polyacrylamide and the preparation method and application thereof

The present invention discloses a novel high-temperature visual acid etching test device and method; the test device includes a visual rock slab holder, an acid solution storage tank I, an acid solution storage tank II, a heating apparatus, a high-pressure water pump, a low-pressure acid pump, a back-pressure valve, an acid valve A, an acid valve B, an acid valve C, an acid valve D, an acid valve E, an acid valve F, a water valve G, a water valve H, a water valve I, a water valve J, and a water valve K; both the acid solution storage tank I and the acid solution storage tank II are provided with a piston therein, where the acid solution storage tank is divided into upper and lower independent parts by the piston. According to the present invention, the flowing process of an acid solution in a fracture can be directly observed to accurately characterize the distribution of the acid solution in the fracture, which facilitates a study on an acid etching mechanism. According to the present invention, an acid solution injection system is separated from a water injection system, so that only water is injected into the system through a high-pressure pump, effectively solving safety problems of acid solution pumping. In the test process of the present invention, a totally-enclosed acid solution system can ensure that the acid solution does not overflow at high temperature and high pressure, thus greatly increasing the safety of the test.

High-temperature visual acid etching experimental device and method

A structural stabilizer for a fiber and proppant complex to enhance proppant migration and placement in a fractured well during propping and a preparation method thereof are provided. The structural stabilizer consists of: water, inorganic salt, kaolinite, nitrogen-doped modified graphene oxide, anionic surfactant, non-ionic alkyl polyglucoside, and polyacrylamide. The structural stabilizer improves bonding between a proppant and a fiber when slick water is used in stimulated reservoir volume (SRV) fracturing, prevents separation of the fiber and the proppant during migration, thereby reducing escape rate of the fiber from the fiber and proppant complex.

Structural stabilizer for fiber and conventional proppant complex in efficient proppant migration and placement technology of fractured well and preparation method

A soluble metal sealing ring with a controllable dissolution rate and preparation process thereof include an aluminum alloy sealing ring matrix and a composite coating coated on an outer surface of the aluminum alloy sealing ring matrix whose standard electrode potential is greater than &#x2212;0.3 volts (V). The preparation process includes: (1) preparing a high-plastic aluminum alloy; (2) preparing the aluminum alloy sealing ring matrix by machining; (3) annealing the aluminum alloy sealing ring matrix; (4) mixing raw materials of the composite coating evenly; (5) preparing the composite coating on an outer surface of the aluminum alloy sealing ring matrix; (6) preparing holes. The soluble metal sealing ring solves problem that good sealing performance and good dissolving performance are difficult to obtain simultaneously in the existing product, and has advantages of good sealing performance, controllable dissolving rate, no blockage and others.

Soluble metal sealing ring with controllable dissolution rate and preparation process thereof

A method for characterizing complexity of rock fracture based on fractal dimension and a device thereof are provided. The method includes steps of: collecting rock fracture samples of a rock, and collecting basic parameters of the rock; determining a fractal dimension of a rock fracture morphology of the rock; calculating the fractal dimension of the rock; calculating a complexity coefficient Fc of rock fracture of the rock; and characterizing a complexity of rock fracture of the rock based on the complexity coefficient Fc of rock fracture of the rock. In the present invention, combined with the fractal geometry theory, fracture complexity coefficient of shale rocks is redefined and calculated to accurately characterize rock fracture morphology, so that characteristics of rock fracture morphology is correctly understood and affecting factors of fracture morphology is analyzed.

Method for characterizing complexity of rock fracture based on fractal dimension and device thereof

The present invention discloses a numerical simulation method for proppant transport considering wall-retardation effect, comprising the followings: establish a physical model of laboratory experiment on proppant transport with a large flat-panel device; establish a drag coefficient model considering wall-retardation effect according to the numerical simulation experiment; establish a computational geometric model; set boundary conditions and physical parameters of the geometric model according to the two-fluid simulation method for solid proppant quasi-fluidization; verify the grid independence of the computational geometric model to obtain the transport characteristics and placement pattern of the proppant in fractures. The present invention employs a numerical simulation method to study the migration and distribution patterns of proppant under the retardation effect of narrow walls during the hydraulic fracturing. The method is reliable in principle and can accurately predict proppant transport in subsurface hydraulic fractures with consideration of the wall-retardation effect on proppant transport.

Numerical simulation method for proppant transport considering wall-retardation effect

A method for determining sand pumping parameters based on width distribution of fracture, including: acquire basic parameters of a target reservoir, simulate a propagation of the fracture, and obtain a propagation pattern and width distribution of the fracture; determine a maximum proppant particle size for entering the fracture at all width levels according to statistical results of the width distribution of the fracture; determine a multi-size combination of proppants according to a mapping table for particle size vs mesh of proppants, and determine an initial ratio of the proppant with each particle size; conduct a numerical simulation of proppant transportation in the fracture to determine a retention ratio of the proppants with each particle size; correct the initial ratio of the proppants with each particle size; calculate an amount of the proppants with each particle size according to the final ratio and the sand pumping intensity and fracturing interval length.

Method for determining sand pumping parameters based on width distribution of fracture

An injection method for a solid retarded acid includes mixing a solid acidic substance with a natural polymer, extruding through an extruder to produce particles; putting the produced particles in a coating pan, and sprinkling zinc acetate powder; turning on the coating pan to rotate while irradiating with an infrared lamp; spraying a glycolic acid aqueous solution with a spray gun, and continuing to rotate to obtain the solid retarded acid; injecting non-reactive liquid and the solid retarded acid into the a sand mixing truck; after the mixture is uniformly mixed in the sand mixing truck, injecting the mixture into a formation by a fracturing truck; conveying the solid retarded acid to a designated location, then stopping a pump, removing pipelines, and opening the well for gushing. The method is good in drag reduction, easy for flowback, thereby reducing the construction cost and facilitating environmental protection, and has broad application.

Injection method for solid retarded acid

The present invention discloses a method for experimentally determining the influence of acid liquor on the Young modulus of compact carbonate rock. The method comprises the following steps: (1), selecting a standard core of compact carbonate rock for use, carrying out a uniaxial compressive strength experiment to establish an empirical relationship between the uniaxial compressive strength and the Young modulus of the compact carbonate rock; (2), selecting a full-diameter core in a target work area for use, carrying out a rock scratching experiment by using a rock scoring instrument, testing the compressive strength of the core, and acquiring the Young modulus of the core before acid treatment; (3), soaking the acid liquor and the core in a high-temperature and high-pressure reactor for a soaking reaction; and (4), carrying out a scratching experiment again on the core soaked with the acid liquor in the original scratching experiment position, testing the compressive strength of the core, acquiring the Young modulus of the core after acid treatment, and determining the influence of the acid liquor on the Young modulus of the compact carbonate rock. The method disclosed by the present invention is reliable in principle, and simple and convenient in operation. The influence of the acid liquor on the Young modulus of the compact carbonate rock under reservoir conditions is authentically evaluated, and the acid fracturing transformation effect of the compact carbonate rock is further improved.

Method for experimentally determining influence of acid liquor on Young's modulus of compact carbonate rock

The invention discloses a testing device and method for evaluating effects of COreaction rate of acid rock plate. The testing device includes an acid fluid conveying unit, a COconveying unit, a mixing tank, a plate holder, a recycling fluid tank, and a vacuum pump. The mixing tank includes an acid fluid inlet, a COinlet, and a miscible fluid outlet. The acid fluid inlet is connected with the acid fluid conveying unit, the COinlet is connected with the COconveying unit, the miscible fluid outlet is connected with the plate holder, the plate holder is connected with the recycling fluid tank, and the recycling fluid tank is connected to the vacuum pump. The COconveying unit includes a COcylinder and a gas booster pump which is connected to the cylinder. The outlet of the pump is connected to the gas inlet of the mixing tank.

Testing method for evaluating the effect of CO2 reaction rate of acid rock plate

The invention introduces a method of calculating etching profile of acid-etched fracture system considering complex filtration media, which mainly considers dynamic filtration caused by natural fractures and acid-etched wormholes in acid fracturing, calculates the above filtration process by a numerical method, and finally calculates acid etching profile of acid-etched fracture system based on acid concentration profile. Calculation equations include fluid pressure in natural fractures, filtration velocity in natural fractures, fracture geometry of hydraulic fractures, fluid pressure in matrix rock, acid concentration profile in natural fractures and hydraulic fractures, acid etching width in hydraulic fractures and natural fractures, and length of acid-etched wormhole, etc. The invention is reliable in principle and efficient in calculation, which is also beneficial to accurately calculating fracture etching profiles of acid fracturing in naturally-fractured reservoirs, improving the accuracy of optimizing acid fracturing treatment parameters, and providing guiding significance for acid fracturing optimization of naturally-fractured carbonate reservoirs.

Method of calculating etching profile of acid-etched fracture system considering complex filtration media

A method for determining a favorable time window of an infill well of an unconventional oil and gas reservoir, which comprises the following steps: S1, establishing a three-dimensional geological model with physical properties and geomechanical parameters; S2, establishing a natural fracture network model in combination with indoor core-logging-seismic monitoring; S3, calculating complex fractures in hydraulic fracturing of parent wells; S4, establishing an unconventional oil and gas reservoir model and calculating a current pore pressure field; S5, establishing a dynamic geomechanical model and calculating a dynamic geostress field; S6, calculating complex fractures in horizontal fractures of the infill well in different production times of the parent wells based on pre-stage complex fractures and the current geostress field; S7, analyzing a microseismic event barrier region and its dynamic changes in infill well fracturing; and S8, analyzing the productivity in different infill times, and determining an infill time window.

Method for determining favorable time window of infill well in unconventional oil and gas reservoir

An experimental test method for dynamic imbibition capacity of shale is provided. The method includes the following steps: core preparation; physical parameter test of shale; experimental loading conditions are determined according to formation stress, formation temperature and hydraulic fracturing parameters; and a dynamic imbibition saturation is defined to characterize a dynamic imbibition amount. Various factors, such as fracturing fluid flow, formation confining pressure, formation temperature and fluid pressure, are used to obtain change rules of dynamic imbibition with time under different construction parameters in shale fracturing process.

Method for dynamic imbibition capacity of shale

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Chengdu, China

Jianchun Guo