China University of Petroleum

Jiahao Liang

Rui Zhang

Chunming Xu

Zhichang Liu

Haiyan Liu

Xianghai Meng

Qinghong Wang

Chunmao Chen

Zhongjin Yi

A method and a system for treatment of a spent chloroaluminate ionic liquid catalyst and an alkaline wastewater, where the method includes: 1) mixing the catalyst with a concentrated brine for hydrolysis reaction until residual activity of the catalyst is completely eliminated, to obtain an acidic hydrolysate and an acid-soluble oil; 2) mixing the acidic hydrolysate with an alkaline solution containing the alkaline wastewater for neutralization reaction until this reaction system becomes weak alkaline, to obtain a neutralization solution; 3) fully mixing the neutralization solution with a flocculant, carrying out sedimentation and separation, collecting the concentrated brine at an upper layer for reuse in the hydrolysis reaction, and collecting concentrated flocs at a lower layer; 4) dehydrating the concentrated flocs to obtain concentrated brine for reuse into the hydrolysis reaction, and collecting a wet solid slag; and 5) drying the wet solid slag to obtain a dry solid slag.

Method and system for treatment of spent chloroaluminate ionic liquid catalyst and alkaline wastewater

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Beijing, China

Jiahao Liang