Forschungszentrum Juelich Gmbh

Forschungszentrum Julich Gmbh

Jesus Gonzalez

Robert Vassen

Olivier Guillon

Martin Bram

Apurv Dash

Robert VAßEN

Diana Marcano

The invention relates to a method for producing a non-oxide ceramic powder comprising a nitride, a carbide, a boride or at least one MAX phase with the general composition Mn+1AXn, where M=at least one element from the group of transition elements (Sc, Ti, V, Cr, Zr, Nb, Mo, Hf and Ta), A=at least one A group element from the group (Si, Al, Ga, Ge, As, Cd, In, Sn, Tl and Pb), X=carbon (C) and/or nitrogen (N) and/or boron (B), and n=1, 2 or 3. According to the invention, corresponding quantities of elementary starting materials or other precursors are mixed with at least one metal halide salt (NZ), compressed (pellet), and heated for synthesis with a metal halide salt (NZ). The compressed pellet is first enveloped with another metal halide salt, compressed again, arranged in a salt bath and heated therewith until the melting temperature of the salt is exceeded. Optionally, melted silicate can be added, which prevents the salt from evaporating at high temperatures. Advantageously, the method can be carried out in the presence of air.

Method for producing non-oxide ceramic powders

A method for sintering metallic and/or non-oxide components includes completely encapsulating, in a metal halide salt, a green body comprising at least one metallic and/or non-oxide powder, and compressing the encapsulated green body so as to be gastight. The method further includes heating, together with a metal halide salt in the presence of oxygen up to sintering temperatures, the compressed, encapsulated green body. The method additionally includes at least partially dissolving, after cooling, the metal halide salt in a liquid so that the sintered component can be removed.

Method for sintering metals, non-oxide ceramics and other oxidation-sensitive materials

Disclosed is a method for producing a metal or ceramic component having regions of differing porosities. The method includes subjecting powder or a presintered precursor to a pressure-assisted pressing and sintering step, using at least one punch for the pressing step. The at least one punch has a contact surface that is intended for making contact with the powder or the presintered precursor and that has a flat outer region and an inner region having a concave recess. After the sintering step, a component is obtained that has a flat outer compacted region having a first porosity and an inner porous region having a second porosity. The component has, on at least one side, a defined transition region between the outer region and the inner region.

Method for producing metal or ceramic components and components

Growing community of inventors

Aachen, Germany

Jesus Gonzalez