Commissariat a L'energie Atomique Et Aux Energies Alternatives

Jean-François Henne

Valérie Chaumat

Nadia Miloud-Ali

Fiqiri Hodaj

Valerie Chaumat

A method is described for assembling at least two parts made of silicon carbide based materials by non-reactive brazing in an oxidizing atmosphere, each of the parts comprising a surface to be assembled, wherein the parts are placed in contact with a non-reactive brazing composition, the assembly formed by the parts and the brazing composition is heated to a brazing temperature sufficient for completely or at least partially melting the brazing composition, or rendering the brazing composition viscous, and the parts and the brazing composition are cooled so as to form, after cooling the latter to ambient temperature, a moderately refractory joint. The non-reactive brazing composition is a composition A consisting of silica (SiO), alumina (AlO), and calcium oxide (CaO), or a composition B consisting of alumina (AlO), calcium oxide (CaO), and magnesium oxide (MgO), and, before heating the assembly formed by the parts and the brazing composition to the brazing temperature, a supply of silicon in a non-oxidized form is carried out on the surfaces to be assembled of the parts to be assembled, and/or on the surface layers comprising the surfaces to be assembled of the parts to be assembled, and/or in the brazing composition.

Method for assembling parts made of SiC materials by means of non-reactive brazing in an oxidizing atmosphere, brazing compositions, and gasket and assembly obtained by said method

A method for joining, assembling, at least two parts made of silicon carbide-based materials by non-reactive brazing is provided. According to the method, the parts are contacted with a non-reactive brazing composition, the assembly formed by the parts and the brazing composition is heated to a brazing temperature sufficient to melt the brazing composition totally or at least partly, and the parts and brazing composition are cooled to that, after solidification of the brazing composition, a moderately refractory joint is formed; wherein the non-reactive brazing composition is an alloy comprising, in atomic percentages, 45% to 65% silicon, 28% to 45% nickel and 5% to 15% aluminum. A brazing composition as defined above is provided. A brazing paste, suspension comprising a powder of said brazing composition and an organic binder as well as a joint and assembly obtained the foregoing method are also provided.

Compositions for joining and assembling parts made of SiC-based materials

A method for joining, assembling, at least two parts comprising silicon carbide-based materials is provided. The parts are contacted with a non-reactive brazing composition, the assembly having the parts and the brazing composition is heated to a brazing temperature sufficient to melt the brazing composition, and the parts and the brazing composition are cooled so that, after solidification of the brazing composition, a moderately refractory joint is formed. The brazing composition is a binary alloy consisting, in atomic percentages, of 60% to 66% silicon and 34% to 40% nickel. Prior to contacting the parts with the brazing composition, a reinforcement is added. A composition comprising the brazing composition and a reinforcement is provided. A brazing paste, suspension comprising a powder of the brazing composition, a reinforcement, and an organic liquid cement, binder, or an organic viscous gel is provided. A joint and assembly obtained by the foregoing method is provided.

Method for assembling, joining parts made of SiC-based materials by non-reactive brazing with addition of a reinforcement, brazing compositions and joint and assembly obtained by said method

A method for assembling at least two parts made of silicon carbide-based materials by non-reactive brazing is disclosed. The two parts are contacted with a non-reactive brazing composition. The assembly formed by the parts and the brazing composition is heated to a brazing temperature sufficient to melt the brazing composition. The parts and the brazing composition are cooled so that, after solidification of the brazing composition, a moderately refractory joint is formed. The non-reactive brazing composition is a binary alloy composed, in mass percentages, of about 46% to 99% silicon and 54% to 1% neodymium.

Method for assembling parts made of SiC materials by non-reactive brazing, brazing compositions, and joint and assembly obtained by said method

Method for joining, assembling parts made of SiC-based materials by non-reactive brazing, brazing compositions, and joint and assembly obtained by said method

A method for joining, assembling, at least two parts made of silicon carbide-based materials by non-reactive brazing is provided. According to the method, the parts are contacted with a non-reactive brazing composition, the assembly formed by the parts and the brazing composition is heated to a brazing temperature sufficient to melt the brazing composition totally or at least partly, and the parts and the brazing composition are cooled so that, after solidification of the brazing composition, a moderately refractory joint is formed; wherein the non-reactive brazing composition is a binary alloy consisting in atomic percentages, of 60% to 66% silicon and 34 to 40% nickel. A brazing composition as defined above is also provided. A paste, suspension of braze alloy comprising a powder of the brazing composition and an organic binder is provided. In addition, a joint and assembly obtained with the foregoing method is provided.

Method for assembling, joining parts made of SiC-based materials by non-reactive brazing, brazing compositions, and joint and assembly obtained by said method

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Bethune, France

Jean-François Henne