The Badger Company, Inc.

James J Graham

Darrell D Kinzler

Edward P Hunt

Roger J Vernon

The invention provides an improved method and apparatus for operating a fluidized bed chemical processing unit of the type having steam generating coils, so as to reduce the occurrence of thermally-induced stresses in the coils and thereby extend the useful life of the coils. The invention involves causing the tube wall temperature of a coil being brought into service to be lowered from bed temperature prior to initiating water flow in the coil, so as to decrease the thermal shock temperature gradient and thereby reduce the magnitude of thermally-induced stress in the coil. The invention utilizes a base coil in addition to the steam generating coil that is being cycled, and a pair of steam drums which operate at a pressure differential. The method involves generating saturated steam in the base coil and superheating the saturated steam in the coil being brought on line. Steam is directed from one drum to the other in a predetermined manner so as to provide proper temperature control of the coil being cycled.

Process for reducing thermal shock in fluidized bed stem coils cycled in

Steam carrying fatty acids is contacted in a barometric condenser with a cooling medium comprising a fatty acid having between six and eighteen carbon atoms to produce a liquid organic phase containing the fatty acids which were entrained in the steam, and an aqueous phase, such phases being readily separated by decantation. After separation of the phases, a portion of the organic phase is used for the cooling medium.

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Wayland, MA, United States of America

James J Graham