Surface Combustion, Inc.

Owens-illinois, Inc.

James Edward Brug

Ralph Paul Poor

Stephen Harry Verhoff

Garry W Barbee

Gary W Barbee

Eric X Heidelberg

Vacuum carburizing of ferrous workpieces is performed at low pressure in a vacuum furnace using an unsaturated aromatic such as benzene as the carburizing medium. The unsaturated aromatic is gas phase hydrogenated into naphthenes, such as cyclohexane, which is metered into the furnace chamber proper and functions as the carburizing gas. The furnace is constructed to be generally transparent to the naphthenes so that cracking tends to occur at the workpiece which functions as a catalyst to minimize carbon deposits. The unsaturated aromatic is supplied in liquid form to fuel injectors which inject the liquid aromatic as a vapor at duty cycles and firing orders to produce a uniform dispersion of the hydrocarbon gas about the work resulting in uniform carburizing of the workpieces. An in-situ methane infrared sensor controls the process. Excess hydrogen beyond what is required to hydrogenate the aromatic is added to the furnace chamber to either assure full carbon potential and produce methane or to perform variable carburizing. Hydrogenation occurs in a hydrogenation coil in fluid communication with the furnace chamber with temperature for the reaction set by the position of the hydrogenation coil in the furnace insulation.

Furnace for vacuum carburizing with unsaturated aromatic hydrocarbons

Vacuum carburizing of ferrous workpieces is performed at low pressure in a vacuum furnace using a carburizing hydrocarbon as the carburizing medium. The furnace is constructed to be generally transparent to the carburizing hydrocarbon so that cracking tends to occur at the workpiece which functions as a catalyst to minimize carbon deposits. The carburizing hydrocarbon is supplied in liquid form to an injector which injects the liquid carburizing hydrocarbon as a vapor to produce a uniform dispersion of the carburizing hydrocarbon about the workpiece, resulting in uniform carburizing of the workpieces.

Vacuum furnace for carburizing with hydrocarbons

Vacuum carburizing of ferrous workpieces is performed at low pressure in a vacuum furnace using an unsaturated aromatic such as benzene as the carburizing medium. The unsaturated aromatic is gas phase hydrogenated into a napthenes, such as cyclohexane, which is metered into the furnace chamber proper and functions as the carburizing gas. The furnace is constructed to be generally transparent to the napthenes so that cracking tends to occur at the workpiece which functions as a catalyst to minimize carbon deposits. The unsaturated aromatic is supplied in liquid form to fuel injectors which inject the liquid aromatic as a vapor at duty cycles and firing orders to produce a uniform dispersion of the hydrocarbon gas about the work resulting in uniform carburizing of the workpieces. An in-situ methane infrared sensor controls the process. Excess hydrogen beyond what is required to hydrogenate the aromatic is added to the furnace chamber to either assure full carbon potential and produce methane or to perform variable carburizing. Hydrogenation occurs in a hydrogenation coil in fluid communication with the furnace chamber with temperature for the reaction set by the position of the hydrogenation coil in the furnace insulation.

Vacuum carburizing with unsaturated aromatic hydrocarbons

Vacuum carburizing of ferrous workpieces is performed at low pressure in a vacuum furnace using a napthene hydrocarbon as the carburizing medium. The furnace is constructed to be generally transparent to the napthene so that cracking tends to occur at the workpiece which functions as a catalyst to minimize carbon deposits. The napthene is supplied in liquid form to fuel injectors which inject the liquid napthene as a vapor at duty cycles and firing orders to produce a uniform dispersion of the hydrocarbon gas about the work resulting in uniform carburizing of the workpieces. An in-situ methane infrared sensor controls the process. Hydrogen is added to the napthene to either assure full carbon potential and produce methane or to perform variable carburizing.

Vacuum carburizing with napthene hydrocarbons

A method for recovering Tb.sub.4 O.sub.7 from a glass containing terbium oxide is disclosed, the method including the steps of:

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Toledo, OH, United States of America

James Edward Brug