Henkel Corporation

James D Beaulieu

Patrick M McCurry, Jr

Janet R Varvil

Michael W Gibson

Robert L Klein, Jr

Alkyl polyglycoside products having improved color properties are produced by a process which involves reacting a reducing sugar with an alcohol to obtain an alkyl polyglycoside reaction product containing unreacted alcohol which is removed in a thin film evaporator wherein the alkyl polyglycoside product film is contacted by liquid water which cools the film and reduces the amount of color bodies in the product.

Method for making alkyl polyglycosides

A continuous method of bleaching an alkylpolyglycoside, substantially free of alcohol, with peroxy compounds, preferably hydrogen peroxide, which is highly efficient to provide an unexpected high degree of color reduction from a dark brown to a light, white product, from an extinction coefficient color respectively of about 10 to about 15 to about 0.025 to about 0.15. The bleaching is carried out at controlled pH and temperature, under pressure preferably in the presence of Mg or MgO.

Continuous bleaching of alkylpolyglycosides

A continuous method of bleaching an alkylpolyglycoside, substantially free of alcohol, with peroxy compounds, preferably hydrogen peroxide, which is highly efficient to provide an unexpected high degree of color reduction from a dark brown to a light, which product, from an extinction coefficient color respectively of about 10 to about 15 to about 0.025 to about 0.15. The bleaching is carried out at controlled pH and temperature, under pressure preferably in the presence of Mg. The use of a prebleached heel or feed prior to introduction of the unbleached material to be bleached results in a faster approach to equilibrium, steady state, bleaching conditions which results in minimum chemical usage and more rapid production of low color.

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West Chester, OH, United States of America

James D Beaulieu