Honeywell International Inc.

Advansix Resins & Chemicals Llc.

Alliedsignal Inc.

James A Kweeder

Raymond G Wissinger

Alan Bart Levy

Keith Dewayne Cochran

Andrew J Howes

Keith D Cochran

Richard J Williams

Stephanie C Barthe

Gavin Paul Towler

John Armstrong Young

Nancy E Iwamoto

Timothy Gene Holt

Lamberto Crescentini

Arthur Ray Shirley, Jr

Carl John Stevens

Dale A Hangey

Theodore J Jenczewski

Steven Thomas Correale

Ronald Highsmith

David J Loy

Samir Z Abdalla

Terry S Chern

John B Boyle

Maria Anatolyevna Azimova

David Wayne Donnick

Maria A Azimova

Christopher B Pace

Nathan Heldenbrand

Joshua H McGill

Jose Carrazza

Yue Hu

Kenneth D Kunz

Gregory A Cleotelis

Kenneth Kunz

Arthur Ray Shirley

Joshua H Mcgill

David W Donnick

Nancy Iwamoto

Richard Williams

Timothy G Holt

A composition for forming a fiber includes at least one polyamide and caprolactam. The at least one polyamide has a number average molecular weight between 38,000 Da and 100,000 Da. The polyamide is at least partially dissolved in the caprolactam. The caprolactam comprises between 20 wt. % and 90 wt. % of the composition.

Compositions and methods for gel spinning of polyamides

The present technology provides methods and processes of producing ammonium sulfate nitrate 1:2 double salts by combining ammonium sulfate solution, nitric acid and ammonia in an aqueous reaction mixture. The methods include reacting the aqueous reaction mixture, followed by removing water to form the ammonium sulfate nitrate 1:2 double salt.

Method for producing ammonium sulfate nitrate

Ammonium sulfate nitrate double salts may be produced using a process that result in complete or nearly complete conversion to the 2:1 double salt. In some embodiments, the disclosure pertains to methods of controlling moisture content during the production process.

Process for preparing ammonium sulfate nitrate

The present disclosure provides methods for separating ketones and alcohols. In one embodiment, the methods and compositions disclosed are useful in separating cyclohexanol from cyclohexanone. In one embodiment, cyclohexanone is converted to its corresponding oxime by treating the cyclohexanone with hydroxylamine. The resulting cyclohexanone oxime is then separated from the cyclohexanol, providing streams of cyclohexanol and cyclohexanone oxime.

Oximation of KA oil by-product

Fertilizers may include one or more additives that render the fertilizer more resistant to further processing such as thermal processing and/or aqueous-based processing that may otherwise be employed in the attempt to produce explosive materials from the fertilizer. The one or more additives may include materials that increase the chances of detection by providing a visual or olfactory indication of further processing. The one or more additives may include materials that make further processing more difficult or dangerous.

Compositions and methods to detect illicit uses of fertilizers

Compositions and methods to deter illicit uses of fertilizers

Preferred aspects of the present invention provide ammonium nitrate compositions comprising ammonium nitrate and at least one stabilizing agent, and preferably a third compound. In certain preferred embodiments, the stabilizing agent, together with third compound, is present under conditions and in amounts effective to substantially reduce the detonation sensitivity of the composition and/or to otherwise improve a desired property of the composition.

Stabilized compositions comprising ammonium nitrate

Preferred aspects of the present invention provide ammonium nitrate compositions comprising ammonium nitrate and at least a second compound, said second compound being present under conditions and in amounts effective to substantially reduce the detonation sensitivity of the composition and/or to otherwise improve a desired property of the composition. In certain embodiments, the second compound is selected from the group consisting of ammonium sulfate, ammonium phosphate, calcium nitrate, potassium nitrate, magnesium nitrate, ammonium molybdenate, ammonium hexaflouralsilicate, neodymium hydroxynitrate, and combinations of two or more of these. In preferred embodiments, at least a substantial portion of the ammonium nitrate in the composition is in the form of a double salt with one or more of said second compounds. In highly preferred embodiments, the present compositions consist essentially of one or more double salts of ammonium nitrate and a second compound as described herein.

Compositions comprising ammonium nitrate double salts

Methods and apparatus for prilling are provided which include dynamically controlling the pressure at the prill head for increased control over prill quality and size distribution. In one embodiment, the pressure of a headspace above a volume of liquid or slurry is regulated to maintain a more precise control of the pressure of the liquid or slurry at the prill head. In another embodiment, an axial upflow device is used to maintain a more precise control of the pressure of the liquid or slurry at the prill head.

Method and apparatus for prilling with pressure control

A method forms a relatively stable ammonium nitrate composite material. The method includes (a) blending ammonium nitrate with an average particle diameter greater than about 1 mm and a substantially non-oxidizing compound in fine particle form; and (b) reducing the average size of said ammonium nitrate granules in the presence of the non-oxidizing compound in fine particle form to produce a substantially homogeneous blend of ammonium nitrate and the non-oxidizing compound having an average particle diameter of about 1 to about 1,000 &#x3bc;m to form a substantially non-explosive powder.

Weakly oxidizing ammonium nitrate composite materials and methods for preparing such compositions

Methods for the production of ammonium sulfate nitrate include (a) providing at a temperature of less than about 175&#xb0; C. a melt including ammonium nitrate, ammonium sulfate, and water and the water content is greater than about 2 wt % based on the total weight of ammonium nitrate, ammonium sulfate and water in the melt, and (b) solidifying from the melt 1:2 ANS double salt by cooling at least a portion of the melt at a rate of less than about 100&#xb0; C./min.

Methods for preparing compositions comprising ammonium nitrate double salts

A pre-fiber gel material is described herein that includes: a) at least one amide-based and/or polyamide-based composition; and b) at least one lactam gelling agent, wherein the gel composition has sufficient viscosity and sufficient cohesiveness upon the mixing of the at least one amide-based or polyamide-based polymer and the at least one lactam gelling agent that the composition can be spun into a fiber. In addition, methods are provided herein that teach that the production of a pre-fiber gel composition, including: a) providing at least one amide-based compound; b) providing at least one lactam gelling agent; and c) mixing the at least one amide-based polymer and the at least one lactam gelling agent such that there is sufficient viscosity and to sufficient cohesiveness in the composition so that it can be spun into a fiber.

Pre-fiber gel compositions and materials, methods of manufacture and uses thereof

A pre-fiber gel material is described herein that includes: a) at least one amide-based and/or polyamide-based composition; and b) at least one lactam gelling agent, wherein the gel composition has sufficient viscosity and sufficient cohesiveness upon the mixing of the at least one amide-based or polyamide-based polymer and the at least one lactam gelling agent that the composition can be spun into a fiber. In addition, methods are provided herein that teach that the production of a pre-fiber gel composition, including: a) providing at least one amide-based compound; b) providing at least one lactam gelling agent; and c) mixing the at least one amide-based polymer and the at least one lactam gelling agent such that there is sufficient viscosity and sufficient cohesiveness in the composition so that it can be spun into a fiber.

Pre-fiber gel materials and compositions, methods of manufacture and uses thereof

Modified fertilizer materials are produced, comprising a) at least one fertilizer granule coated with a dispersant to form at least one fertilizer granule-dispersant particle, b) a dispersant, which comprises at least one agrochemical blended with at least one powder, and c) an overcoating material that is applied to the at least one fertilizer granule-dispersant particle. Methods of producing a modified fertilizer materials comprise: a) providing at least one fertilizer granule, b) providing a dispersant that comprises at least one agrochemical blended with at least one powder, c) providing an overcoating material, d) applying the dispersant to the at least one fertilizer granule to form at least one fertilizer granule-dispersant particle, and e) applying the overcoating material to the at least one fertilizer granule-dispersant particle to form the modified fertilizer material.

Chemically and physically modified fertilizers, methods of production and uses thereof

Growing community of inventors

Chesterfield, VA, United States of America

James A Kweeder