Societe Prolabo

Prolabo

Jacques Paturat

Patrick Jacquault

Roland Dequin

Jean-Louis Millet

Jean-Louis Di Martino

Gilles Bart

A chemical reaction is carried out by the wet method on a succession of samples. The chemical reaction is carried out within a reaction chamber which is connected to a fluid-conducting circuit. The reaction chamber is positioned within a microwave cavity. A predetermined quantity of sample is fed into the circuit upstream of the reaction chamber. At least one reactant is introduced into the circuit upstream of the reaction chamber. The reaction chamber, with the sample and reactant disposed therein, is heated by the application of microwaves for a predetermined time. The product of the reaction is recovered. The circuit is then rinsed with a rinsing liquid, and the steps are repeated on the remaining samples.

Microwave chemical reactor for sample analysis

A dissolution cell for determining the kinetics of dissolution of a solid substance in a particular liquid, includes (a) a housing receptacle having a closed bottom end and an open top end, an interior of such receptacle defining (i) a lowermost upwardly diverging conical zone provided with liquid inlet means extending from a tip of the conical zone through the bottom end of the receptacle, (ii) a first essentially cylindrical zone surmounting the conical zone and (iii) a second essentially cylindrical zone surmounting the first essentially cylindrical zone, having a cross-sectional diameter greater than that of the first essentially cylindrical zone and being in communicating relationship therewith, such conical zone (i) and such first essentially cylindrical zone (ii) defining a chamber for the dissolution of a solid substance in a liquid solvent, (b) a closure leak-proofedly secured to the open end of the receptacle and provided with a solute outlet means, and (c) filtration means secured between such closure and an area of communicating relationship between the first and the second essentially cylindrical zones, so as to be disposed in a pathway for the solute extending from the dissolution chamber to the solute outlet means.

Dissolution cell and apparatus for determining solids-dissolving kinetics

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Briare, France

Jacques Paturat