Korea Atomic Energy Research Institute

Korea Hydro Nuclear Power Co., Ltd.

Hye-Ryun Cho

Euo Chang Jung

Kyuseok Song

Jei-Won Yeon

Euo-Chang Jung

Wan-Sik Cha

Kyoung Kyun Park

According to the present invention, there is provided a method of determining a concentration of uranium including: a) a primary measuring step of measuring luminescence intensity or luminescence attenuation of uranium (VI) of an oxidant added sample obtained by adding an oxidant composition to a detection target sample; b) a secondary measuring step of adding different volumes of standard solution containing uranium (VI) having a predetermined concentration to a plurality of oxidant added samples, respectively, and then measuring luminescence intensity or luminescence attenuation of uranium (VI) contained in each standard solution added sample; and c) a calculating step of calculating a concentration of uranium (VI) contained in the detection target sample by a standard addition method based on the primary and secondary measurements. With the method for determining a concentration of uranium according to the present invention, the concentration of uranium may be further rapidly and accurately analyzed.

Uranium analysis using luminescence enhancing oxidant and oxidant composition

Disclosed herein is a method of quantitatively analyzing uranium in an aqueous solution, the method comprising measuring Raman scattering intensity of water and luminescence intensity of uranium standard solutions having various concentrations (Operation 1); calculating a ratio of the uranium luminescence intensity to the Raman scattering intensity of water for each uranium concentration and plotting a calibration curve therethrough (Operation 2); and measuring Raman scattering intensity of water and uranium luminescence intensity of an unknown sample, calculating a ratio of the measured intensities and determining a uranium concentration thereof by using the calibration curve (Operation 3). When the quantitative analysis method of uranium in an aqueous solution according to the present invention is used, inconvenience of a typical analysis method, in which repetitive measurements of calibration curves are required according to various measurement conditions, may be removed.

Method of quantitatively analyzing uranium in aqueous solutions

The present invention relates to an apparatus and method for measuring the size of nanoparticles present in an aqueous solution as an infinitesimal quantity, and, more particularly, to a scheme that remotely measures the laser-induced breakdown of a fine nanoparticle using a probe beam in a non-contact manner, performs curve fitting on the symmetrical frequency distribution curve of the measured magnitude of a probe beam signal to form the shape of a Gaussian function, obtains calibration curves for the size of the nanoparticle from the peak and full-width at half-maximum thereof, and determines the size of an unknown nanoparticle from the calibration curves.

Apparatus for measuring magnitude of deflected probe beam signal generated by laser-induced breakdown and method of measuring size of nanoparticles using frequency distribution curve of magnitude of probe beam deflection signal

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Daejeon, South Korea

Hye-Ryun Cho