The Procter Gamble Company

Hossam Hassan Tantawy

Adam Porter

Nigel Patrick Somerville Roberts

Eric San Jose Robles

Larry Savio Cardozo

James Robert Lickiss

Alan Thomas Brooker

David William York

Helen Amy Lang

Paul Anthony Gould

Andres Arturo Martinez-Guzman

Hossein Ahmadian

Andre Chieffi

Simon Howe

Anthony McMeekin

Nigel Patrick Somerville-Roberts

Jill Robyn Dorgan

William Alexander Caufield

Andrew Brian Greenaway Patton

Stuart Andrew Caldwell

Nicholas Alexander Jesse Mcguckin

Sabrina Beatrice Danielle Gault

Timothy Bullivant

Jose Rodel Mabilangan Caragay

Fatema Amen Abdelhalem Mohamed Beder

Ahmed Ibrahim Sayed Ahmed

Yara Tarek Mohamed Mahdally

Andre-Brian Greenaway Patton

Colin Ure

Carly Pickering

Zoe Dyter

Linsey Sarah Fuller

Victor Stuart Reid

Craig Adam Wilkinson

Stephen John Walker

Christopher Charles Driffield

Matthew Grady McGoff

Joss Prest

Claire Louise Duckitt

David James Parmley

Laura Judith Smalley

Michael Richard Irvine

Scott Edward Stephans

Benjamin Mark Haddrell

Anthony Mcmeekin

Urwin Harrogate

An example system comprises a water-soluble unit dose article comprising a water-soluble fibrous non-woven sheet and a granular laundry detergent. The water-soluble fibrous non-woven sheet is shaped to form a partially sealed internal compartment and has an air permeability comprised between 5 m/m/min and 200 m/m/min. The granular laundry detergent is comprised within said internal compartment and comprises a plurality of particles, wherein the plurality of particles comprises zeolite particles. The system comprises sealing jaws, wherein at least one of the sealing jaws is a heated sealing jaw, wherein a bottom seal of the internal compartment is sandwiched between the jaws. The jaws comprise a non-stick coating in contact with the bottom seal and a first dust extraction conduct to direct a gas flow away from an area surrounding a top section of the sealing jaws or away from a bottom section of the internal compartment.

Dust extraction conducts and processes

An example system comprises a water-soluble unit dose article comprising a fibrous non-woven sheet shaped to form a sealed internal compartment and a granular laundry detergent comprised within the internal compartment. The sheet comprises fibres which comprise polyvinyl alcohol polymer. The granular laundry detergent comprises perfume particles. The system also comprises sealing jaws, whereby at least one of the sealing jaws is a heated sealing jaw. A top seal of the internal compartment is sandwiched between the jaws. A first of said jaws comprises a protruding portion along a longitudinal direction of the seal. The protruding portion has a base along a direction perpendicular to the longitudinal direction of the seal. The base has a dimension of more than 3 times and of less than 20 times a thickness of the water-soluble fibrous non-woven sheet.

Sealing jaws and water-soluble unit dose article comprising a fibrous non-woven sheet

A water-soluble unit dose article including a water-soluble fibrous non-woven and a method of using the water-soluble unit dose article.

Water-soluble unit dose article

A process for making a particulate laundry detergent composition, the process includes the steps: (a) contacting water, starch, acid and perfume to form a concentrated aqueous acidic mixture, the concentrated acidic mixture includes: (i) from about 20 wt % to about 60 wt % starch; (ii) from about 10 wt % to about 50 wt % acid; (ii) from about 2 wt % to about 20 wt % perfume; (iv) from 10 wt % to less than about 45 wt % water; the concentrated acidic mixture has a pH of less than about 4.5; (b) subjecting the concentrated acidic mixture to a perfume emulsification step to emulsify the perfume to form an emulsified perfume mixture in fluid form; and (c) spraying the emulsified perfume mixture in fluid form onto base detergent particles so that the emulsified perfume mixture at least partially coats the base detergent particles to form the particulate laundry detergent composition, the base detergent particles include from about 4 wt % to about 60 wt % detersive surfactant.

Process for making a particulate laundry detergent composition

The present invention relates to a process for preparing a solid free-flowing particulate laundry detergent composition, wherein the process includes the steps of: (a) forming a mixture by contacting: (i) molten fatty acid; (ii) liquid alkaline ingredient, and (iii) non-ionic surfactant, to obtain a mixture, wherein the mixture includes: (i) partially neutralized fatty acid component; (ii) non-ionic surfactant; and (iii) water, wherein the molar ratio of fatty acid to liquid alkaline ingredient contacted together in step (a) is above 1:1; (b) contacting the mixture obtained in step (a) to a detergent powder to form a solid free-flowing particulate laundry detergent composition, wherein in step (b) the mixture is contacted to the detergent powder by spraying the mixture at a temperature of greater than 50° C. onto the detergent powder, wherein the detergent powder includes a detergent ingredient.

Process for making a laundry detergent composition

The present invention relates to a process for preparing a spray-dried laundry detergent particle, wherein the process includes the step of contacting water-insoluble silicate salt to monomeric organic carboxylic acid in an aqueous mixture, wherein the aqueous mixture has a pH of 4.2 or less, wherein the aqueous mixture includes detersive surfactant, wherein the aqueous mixture is substantially free of carbonate salt, wherein the water-insoluble silicate salt reacts with the monomeric organic carboxylic acid to form silica, wherein the aqueous mixture is spray-dried to form a spray-dried laundry detergent particle, wherein the particle comprises: detersive surfactant; monomeric organic carboxylic acid; and silica, wherein the particle is substantially free of carbonate salt.

Process for preparing a spray-dried laundry detergent particle

The present invention relates to a process for preparing a spray-dried laundry detergent particle, wherein the process includes the step of contacting zeolite to monomeric organic carboxylic acid in an aqueous mixture, wherein the aqueous mixture has a pH of 4.2 or less, wherein the aqueous mixture includes detersive surfactant, wherein the aqueous mixture is substantially free of silicate salt, and wherein the aqueous mixture is substantially free of carbonate salt, wherein the zeolite reacts with the monomeric organic carboxylic acid to form silica, wherein the aqueous mixture is spray-dried to form a spray-dried laundry detergent particle, wherein the particle includes: detersive surfactant; monomeric organic carboxylic acid; and silica, wherein the particle is substantially free of silicate salt, and wherein the particle is substantially free of carbonate salt.

A solid free-flowing particulate laundry detergent composition comprising: (a) from 0.1 wt % to 5 wt % hueing agent particle comprising: (i) from 2 wt % to 10 wt % hueing agent, wherein the hueing agent has the following structure: wherein:

Solid free-flowing particulate laundry detergent composition

A solid free-flowing particulate laundry detergent composition including: (a) from 0.1 wt % to 5 wt % polymer particle comprising: (i) from 70 wt % to 90 wt % co-polymer and (ii) from 10 wt % to 30 wt % salt; and (b) from 35 wt % to 80 wt % spray-dried particle including: (i) from 8 wt % to 24 wt % alkyl benzene sulphonate anionic detersive surfactant; (ii) from 5 w % to 18 wt % silicate salt; (iii) from 0 wt % to 10 wt % sodium carbonate; and (iv) from 0 wt % to 5 wt % carboxylate polymer.

A process of making a granular detergent composition comprising the steps of:

Method of making granular detergent compositions comprising polymers

Method of making granular detergent compositions comprising surfactants

The present invention is to a laundry detergent powder comprising: (i) from 20 to 80 wt % of a first particle comprising less than 55 wt % sulphate, anionic detersive surfactant, and having a bulk density of from 300 g/l to 1100 g/l: and (ii) from 20 to 80 wt % of a second particle comprising at least 55 wt % sulphate and, having a bulk density of from 350 g/l to 600 g/l, and a process to making the laundry detergent powder.

Laundry detergent compositions

The present invention is a spray-dried powder comprising: (i) from 20 to 80 wt % of a first spray-dried particle comprising less than 5 wt % sulphate, anionic detersive surfactant and having a bulk density of from 300 g/l to 450 g/l: and (ii) from 20 to 80 wt % of a second spray-dried particle comprising at least 45 wt % sulphate, 0 wt % to 15 wt % anionic detersive surfactant, and having a bulk density of from 350 g/l to 700 g/l.

Spray-dried detergent powder

The present invention is to a process for preparing a spray-dried detergent powder comprising: (a) forming an aqueous detergent slurry in a mixer; (b) transferring the aqueous detergent slurry from the mixer to a pipe leading through a first pump and then through a second pump to a spray nozzle; (c) contacting a liquid detergent ingredient having a viscosity of less than 2 Pa&#xb7;s to the aqueous detergent slurry in the pipe after the first pump and before the second pump to form a mixture; (d) spraying the mixture through the spray nozzle into a spray-drying tower; and (e) spray-drying the mixture to form a spray-dried powder, wherein a nitrogen-rich gas is introduced between the first and second pumps.

Spray-drying process

Growing community of inventors

Northumberland, United Kingdom

Hossam Hassan Tantawy