Jiangnan University

Dongtai Haorui Biotechnology Co., Ltd.

Wuxi Jinshun Lighting Technology Co., Ltd.

Haijun Wang

Yongmei Xia

Yun Fang

Chunyan Wu

Wenwen Yuan

Yi Huang

Xiang Liu

Jing Wu

Liping Zhang

Fei Xu

Xueyi Hu

Liping Zhu

Ye Fan

Zhuoyu Zhou

Guangzhi Xu

Chen Liu

The disclosure discloses a method to elevate the amount of steviol glycosides remained in the recrystallization mother liquor ofextract, and belongs to the field of modification and extraction of natural compounds. The disclosure adopts lactase for highly specific catalytic hydrolysis of stevioside to convert stevioside into rubusoside which usually can only be obtained from leaves ofS. Lee; and meanwhile, after stevioside in the mother liquor glycosides is converted, since the polarity difference between rubusoside and rebaudioside A is far larger than the polarity difference between stevioside and rebaudioside A, rebaudioside A is more easily separated out of the mother liquor glycosides. A technology provided by the disclosure is also applicable to value increment of mixed steviol glycosides containing stevioside and is beneficial for separating out rebaudioside A from the mixed steviol glycosides.

Method to elevate the amount of steviol glycosides remained in the recrystallization mother liquor of Stevia extract

The invention discloses a coordination type zirconium phosphotungstate catalyst and its application in catalytic hydrogenation of furfural, belonging to the field of heterogeneous catalysis. The zirconium phosphotungstate catalyst prepared by the invention not only has good catalytic effect on the conversion of furfural to furfuryl alcohol, but also has mild reaction conditions. The yield of solid line furfuryl alcohol can be 98% if it can be reacted for 1 h at 120 ° C., and the amount of catalyst is less, which greatly reduces the energy consumption in the prior art. In addition, the zirconium phosphotungstate prepared by the invention is easy to separate, has good stability for catalyzing the hydrogenation of furfural to furfuryl alcohol, and is a new, efficient and green catalyst.

Coordination zirconium phosphotungstate catalyst and its application in catalytic hydrogenation of furfural

The present invention discloses a method for preparing glucosyl steviol glycosides through enzymatic catalysis under programming temperatures in high throughput, belonging to the technical field of biosynthesis of sweeteners. By using cyclodextrin glucosyltransferase fromsp. as a catalyst, steviol glycosides as the glycosyl receptor and dextrin or oligosaccharide as the glycosyl donor, taking a calcium/barium ion salt bridge as the main stabilizer and combining with glycerol to adjust the conformation and binding domain openness of the enzyme, and utilizing transglucosylation and hydrolytic activities of amylase at variable temperatures in different stages, thereby preparing the glucosyl steviol glycosides through enzymatic catalysis under programming temperatures in high throughput. The technology of the present invention can improve the utilization rate of the enzyme, and obtain glucosyl steviol glycosides with good sweetness and good taste.

High-throughput enzymatic preparation of glucosylated steviol glycosides under programming temperatures

The present disclosure discloses an immobilized metalloporphyrin catalyst and its utilization in maleic acid preparation, belonging to the technical field of metalloporphyrin catalytic application. The immobilized metalloporphyrin catalyst is used for catalyzing furfural to prepare maleic acid and is good in catalytic effect, mild in reaction conditions and capable of greatly reducing the energy consumption required in the prior art. The catalyst disclosed by the present disclosure can provide a good microenvironment for a reaction, so that the yield and selectivity of maleic acid are increased; and according to a method disclosed by the present disclosure, the conversion ratio of furfural is 20.4%-95.6%, the yield of maleic acid is 10%-56.1%, and the selectivity is 43.6%-76.1%. Meanwhile, the catalyst is easy to separate and environmentally friendly and may be recycled for many times.

Immobilized metalloporphyrin catalyst and its utilization in maleic acid preparation

The present disclosure discloses the preparation and application of magnetic metallic oxide cross-linked acidic polyionic liquid, belonging to the technical field of solid acid catalysis. The catalyst prepared by the present disclosure has good Lewis acid site and Br&#xf6;nsted acid site, and has the characteristics of high speed, high efficiency, environment friendliness and the like when catalyzing preparation of furfural from xylose. The catalyst has the advantages of easy separation, multiple cycles of recycling and the like, and is green and pollution-free. The magnetic metal oxide cross-linked acidic polyionic liquid prepared by using the present disclosure has the characteristics of high speed, high efficiency, environment friendliness and the like when catalyzing preparation of furfural from xylose, and meanwhile, the catalyst has the advantages of easy separation, multiple cycles of recycling and the like, and is green and pollution-free.

Preparation and application of magnetic metallic oxide cross-linked acidic polyionic liquid

The present invention belongs to the technical field of high-power LED lamps, and relates to a high-power LED lamp with a heat dissipation effect, including a shell body. The shell body includes a heat sink main body and a heat sink cover board covering on a back surface of the heat sink main body. A plurality of heat pipes are embedded between the heat sink main body and the heat sink cover board, and an LED chip is placed on a front surface of the heat sink main body. The position of the heat sink main body where the LED chip is placed is the chip heat collecting area, all the heat pipes pass under the chip heat collecting area, and are in close contact with the chip heat collecting area.

High-power LED lamp with heat dissipation effect

The present invention provides a method to produce RD by using a cutinase to catalyze the esterification of RB under stepwise cooling temperatures, which is related to the field of biosynthesis of organic compounds. The method uses a cutinase fromto catalyze the esterification of RB and sophorose to produce RD. The stepwise cooling temperatures are used to reduce the heat inactivation of the enzyme as well as to improve the mass transfer. The method catalyzes the esterification of RB to produce RD in a solvent such as methanol, DMSO and DMF. The reaction is safe, efficient and highly selective. In addition, the method uses stepwise additions of substrate RB and cooling temperatures for the esterification reaction. In this way, it speeds up the initial reaction rate, increases the amount of solved RB as it is converted to RD, and improves the mass transfer to further increase the reaction speed. In summary, the method uses moderate reaction conditions, and has a high yield and a simple purification procedure.

Growing community of inventors

Wuxi, China

Haijun Wang