International Business Machines Corporation

Finings Co. Ltd.

Shanghai Fanglun New Material Technology Co., Ltd.

Guohua Li

Qi Liang

Nongyue Wang

Qi Ye

Tian Tian

Weixiong Rao

Quanzhong Zhao

Jianming Shao

Guoqiang Wen

Xiongwei Qu

In one embodiment of the present disclosure, an original graph including nodes is obtained. The nodes of the original graph are reordered to generate a reordered graph. Non-zero elements in an adjacency matrix for the reordered graph are clustered as compared with an adjacency matrix for the original graph. The adjacency matrix for the reordered graph is encoded with integers. The integers correspond to non-empty blocks in the adjacency matrix for the reordered graph.

Directed graph compression

A method for preparing chlorine gas through catalytic oxidation of hydrogen chloride is carried out by one-time hydrogen chloride feeding and multi-stage oxygen feeding, one-time oxygen feeding and multi-stage hydrogen chloride feeding, or both, returning a product gas stream without separation thereof, and optionally carrying out heat insulation means. In the present invention, excessive reaction heat concentration is prevented, therefore, the method of the present invention is a chlorine gas recovery method implemented through the Deacon catalytic oxidation of hydrogen chloride that may be industrialized.

Method for preparing chlorine gas through catalytic oxidation of hydrogen chloride

Clean process for preparing a chloroformyl-substituted benzene by oxidation of a tail gas hydrogen chloride from a chlorination reaction and a chloroacylation reaction and recycling of the resulting oxidation product chlorine gas into the chlorination reaction. The present invention provides a clean process for preparing a polymer-grade chloroformyl-substituted benzene.

Clean process for preparing chloroformyl-substituted benzene

The present application relates to a method for photochlorination, and specifically to photochlorination by a photochemical reaction of an aromatic compound with gaseous chlorine so as to prepare a trichloromethyl-substituted benzene, and to a method using bis-(trichloromethyl)-benzene as the trichloromethyl-substituted benzene to prepare by further reaction bis-(chloroformyl)-benzene. Through the control of temperature, illuminance and consumption of gaseous chlorine, the method of this application can greatly improve the purity of trichloromethyl-substituted benzene and further prepare polymer-grade bis-(chloroformyl)-benzene with low cost. The present application also relates to a method for purifying trichloromethyl-substituted benzene, and specifically to a method for purifying trichloromethyl-substituted benzene via molecular distillation. The present application further relates to a photochlorination reactor for use in photochlorination reactions (such as those of the present application).

Method for the preparation of trichloromethyl-group-substituted benzene

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Shanghai, China

Guohua Li