A E Staley Manufacturing Company

Novo Nordisk A/s

Novozymes A/s

Ensyn Renewables, Inc.

Gin C Liaw

Allan Svendsen

Sven Pedersen

Hanne Vang Hendriksen

Munir Cheryan

Ruby Illum Nielsen

Roger S Leiser

Bjarne Ro Nielsen

Barry A Freel

James M Gaddy

Roy O Elmore

Bjarne R&oslash;nfeldt Nielsen

Charles E Schollmeier

Steven J Reust

Cameron Ferguson

Frank M Mallee

Eric H Lutz

A method of producing activated carbon comprising the steps of a) pyrolysing corn derivatives to generate char and b) activating the char to produce activated corn carbon.

Process for producing activated carbon

An improved corn wet milling process is disclosed in which a first stream comprising water, starch, and protein (e.g., gluten) is generated by separating fiber from wet milled de-germed corn particles (e.g. fiber separation step). Membrane filtration (e.g. starch-protein stream thickening) is performed on the first stream, producing a first retentate and a first aqueous permeate. The first retentate (e.g. thickened starch-protein stream) is separated into a second stream and a third stream (e.g. primary starch separation step). The second stream comprises water and a majority of the starch present in the first retentate, and the third stream comprises water and a majority of the protein (e.g., gluten) present in the first retentate. This process provides an economical means of recovering a higher percentage of the available cornstarch for inclusion in high value products.

Membrane filtration for thickening and starch washing in corn wet milling

The present invention relates to a method for the production of saccharide preparations, i.e., syrups, by saccharifying a liquefied starch solution, which method comprises a saccharification step during which step one or more enzymatic saccharification stages takes place, and the subsequent steps of one or more high temperature membrane separation steps, and re-circulation of the saccharification enzyme, in which method the membrane separation steps are carried out as an integral part of the saccharification step. In another specific aspect, the invention provides a method of producing a saccharide preparation, which method comprises an enzymatic saccharification step, and the subsequent steps of one or more high temperature membrane separation steps and re-circulation of the saccharification enzyme.

Method of producing saccharide preparations

The present invention relates to a method for the production of saccharide preparations, i.e., syrups, by saccharifying a liquefied starch solution, which method comprises a saccharification step during which step one or more enzymatic saccharification stages takes place, and the subsequent steps of one or more high temperature membrane separation steps, and recirculation of the saccharification enzyme, in which method the membrane separation steps are carried out as an integral part of the saccharification step.

An improved corn wet milling process is disclosed. In a process in which corn kernels are steeped in an aqueous solution and are milled to facilitate the separation of the components thereof, in which starch from the corn is separated from gluten, and in which at least one aqueous gluten-containing stream is generated, the improvement comprises membrane filtration of an aqueous gluten-containing stream, producing a gluten-enriched retentate, and removing water from the gluten-enriched retentate, thereby producing a substantially dry gluten product. This improved process provides an economical means of recovering a higher percentage of the available protein for inclusion in high value products.

Process for recovery of protein from aqueous media in corn wet milling

An improved corn wet milling process is disclosed, in which gluten is recovered from steepwater by membrane filtration and is incorporated in a corn gluten meal product. The process can include the steps of steeping corn kernels in an aqueous solution, thereby producing steep water which contains gluten protein; membrane filtration of the steep water, thereby producing a retentate which has a higher concentration of the gluten protein than the original steep water; reducing the water content of the retentate; and incorporating the remaining retentate into a corn gluten meal product.

Process for recovery of insoluble protein from steep water

A method for producing anhydrous crystalline fructose by crystallizing from solution is provided. A highly supersaturated aqueous solution of fructose is added to a heel of crystalline fructose and dry seed. The temperature of the solution is then lowered to crystallize fructose from the solution to form a massecuite. The massecuite is divided into a product portion and a heel portion, the product portion being treated to isolated crystalline fructose which is then classified into product cuts on the basis of particle size of the fructose crystals, each product cut having a substantially typical particle size distribution.

Method for crystallization of fructose

Large-scale apparatus and process for chromatographic separation of fructose/dextrose sugar solutions employing large diameter beds of a strongly cationic salt of an ion exchange resin. The cationic ion exchange resin is densely and uniformly packed in a separation column by means of a resin loading method which includes washing the resin with a salt selected from the group of calcium, barium, strontium or silver salts of the resin. The shrunken resin is then placed in the column to completely fill the column. After sealing the column, excess salt is washed away to thereby expand the resin inside the confined separation column chamber. The uniformly dense packing of the resin in the separation column chamber eliminates the need for mechanical baffles which were formerly required to insure regular and uniform flow throughout the entire cross sectional area of the separation columns. Large diameter separation columns without baffles are made possible by the column packing method of the invention because undesirable channeling or irregular flow in the densely packed resin bed is virtually eliminated. A liquid feed stream containing fructose and dextrose and a second stream of elution water are fed through a series of separation columns in alternate, cyclic pulses. The liquid streams are further redistributed between the successive columns of the series to further increase the degree of separation of the output stream into a portion rich in fructose, and another output stream rich in dextrose.

Process and equipment for chromatographic separation of

Mother liquors obtained from a dextrose crystallization process may be upgraded for re-cycling to dextrose crystallizers by transferring the mother liquor through a bed of an adsorption agent which preferentially adsorbs either dextrose or oligosaccharides. A dextrose-rich portion of the mother liquor is then recovered from either the dextrose-rich fraction which passes through the bed or has been preferentially adsorbed and eluted from the bed with a solvent.

Growing community of inventors

Decatur, IL, United States of America

Gin C Liaw