Ionics, Inc.

Resources Conservation Company

George R Jones

Dan Peterson

Joseph J Bostjancic

Robert L Solomon

Ferris C Standiford

Howard R Herrigel

James C Nowak

Mark K Tose

John E Andrew

Robert Whalen

An improved salt basket for dewatering solids, particularly salts resulting from evaporation of industrial wastewaters. The salt basket system includes a pressurizable vessel having a screen floor situated above a bottom liquid collection head, an inlet for the brine/solids slurry from which solids are to be separated and dried, an inlet for air, an inlet for steam (the latter two inlets may be combined, where convenient), an inlet for solids free feed, and a drain outlet (these two may be combined where convenient into a combination feed/drain connection). Preferably, an automated system for introducing feed brine and for removing the solids product is provided. For safety, a pivotally attached lower door has a hydraulic failsafe closure mechanism and locking safety latches to prevent the door from inadvertently opening. The process control design minimizes exposure of the salt basket interior to supersaturated solutions with precipitating solids therein, thus reducing scaling of the salt basket, by introducing feed brine rather than magma (crystal/concentrated liquor slurry) to the salt basket between crystal harvest cycles.

Salt basket for crystallizer and method of use in zero liquid discharge

The present invention is a method for using water to remove amine from an oil-amine component. The oil-amine component is typically produced in prior art processes using an amine having an inverse critical solution temperature with water to break emulsions and sludges. The steps of the present invention include adding water to the oil-amine component in an amount sufficient to form a water-amine azeotrope with substantially all the amine in the oil-amine component followed by heating to remove the azeotrope. The method of the present invention may be used to remove amine from an oil-amine component even where the amine is present in an amount as low as 10% or less by weight.

Method for removing amine from oil

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Renton, WA, United States of America

George R Jones