Exxonmobil Research and Engineering Company

George Akehurst

Manuel S Alvarez

Limin Song

Alan Mark Schilowitz

Timothy D Shaffer

Pamela Jean Wright

Henry Alan Wolf

H Alan Wolf

James Edward Feather

Dalia Yablon

Chung-Min Cheng

Mechanical oscillators employ the use of resonance parameters, frequency and the quality factor Q, for the measurement of corrosion or deposition. The ability of a mechanical oscillator to measure small amounts of metal loss or deposition is not only dependent upon the mechanical design but is limited by the precision in determining the resonance frequency and Q. Methods for measuring these resonance parameters with a high precision in the presence of noise are provided. The increased degree of precision improves the utility of these devices as sensitive probes for corrosion and deposition (fouling) measurement. The increased degree of precision is enabled in part by employing curve fitting consistent with modeling the mechanical oscillator as a simple harmonic oscillator. This curve fitting procedure, combined with averaging and utilizing signal processing parameters to mitigate noise effects, adds precision in measuring resonance parameters.

Determining the resonance parameters for mechanical oscillators

Method of reducing fouling in an elastomer polymerization process that includes providing a reactor capable of housing an industrial-scale elastomer polymerization reaction, and applying a mechanical force to the reactor so as to create a vibration in at least one wall of the reactor, in which fouling is reduced in the reactor. In one embodiment the reaction is an industrial scale butyl polymerization reaction and the reactor is a butyl polymerization reactor.

Mitigation of elastomer reactor fouling using mechanical vibration

The present invention is a mechanical oscillator for detection and measurement of corrosive foreign materials. The elements include a mechanical oscillator that is mechanically excited, wherein the mechanical oscillator has a resonant frequency, f, and a quality factor, Q. A fuse fixed to the oscillator to change oscillator amplitude to and from essentially zero to resonance amplitude. In a preferred embodiment, the mechanical oscillator has the shape of a tuning fork where one region is compatible with the service fluid and the other region is incompatible with the service fluid or other contaminant. The sensor alarms when a measured amount of the incompatible material has been removed or the physical strength of the material has been compromised.

Mechanical oscillator activated or deactivated by a predetermined condition

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Belvidere, NJ, United States of America

George Akehurst