Mitsubishi Kasei Corporation

Ryoka Techno Engineering & Construction Co.

Mitsubishi Chemical Corporation

Mitsubishi Kasei Engineering Company

Furuto Seiryo

Masaaki Mita

Kenji Sugimoto

Katashi Shioda

Moriyoshi Kudoh

An apparatus for separating a liquid by pervaporation, which comprises at least one pervaporation membrane module unit for purifying a liquid to be treated, a supply line connected to said pervaporation membrane module unit for supplying the liquid to be treated to the membrane module unit, a withdrawing line for withdrawing the permeated fluid from the membrane module unit and a withdrawing line for withdrawing the non-permeated liquid, wherein said supply line is provided with a pressure pump for transporting the liquid and a heater, and the final withdrawing line for the non-permeated liquid is provided with a pressure regulating valve.

Apparatus for separating a liquid mixture

A apparatus for separating water by pervaporation from a liquid mixture comprising isopropanol and water, which comprises (a) heating the liquid mixture, then supplying the heated mixture to a pervaporation membrane module unit using a polyimide-type separating membrane to conduct separation of the liquid mixture, recycling a part or whole of the liquid not permeated through the membrane to a feed liquid mixture, supplying a fresh feed liquid mixture to an optional place in the circulation route, and withdrawing the liquid mixture from an optional place in the circulation route, (b) controlling the amount of the liquid to be recycled among the liquid not permeated through the membrane to a level of at least 10 times by volume the amount of the fresh feed liquid mixture, and (c) controlling the difference between the liquid temperature at the inlet of the membrane module unit and the liquid temperature at the outlet of the membrane module unit to a level of at most 20.degree. C.

Method for separating a liquid mixture

A method for separating water by pervaporation from a liquid mixture comprising isopropanol and water, which comprises (a) heating the liquid mixture, then supplying the heated mixture to a pervaporation membrane module unit using a polyimide-type separating membrane to conduct separation of the liquid mixture, recycling a part or whole of the liquid not permeated through the membrane to a feed liquid mixture, supplying a fresh feed liquid mixture to an optional place in the circulation route, and withdrawing the liquid mixture from an optional place in the circulation route, (b) controlling the amount of the liquid to be recycled among the liquid not permeated through the membrane to a level of at least 10 times by volume the amount of the fresh feed liquid mixture, and (c) controlling the difference between the liquid temperature at the inlet of the membrane module unit and the liquid temperature at the outlet of the membrane module unit to a level of at most 20.degree. C.

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Tokyo, Japan

Furuto Seiryo