Commissariat a L'energie Atomique

Nanomakers

Commissariat &#xc0; L'&#xc9;nergie Atomique Et Aux &#xc9;nergies Alternatives

Francois Tenegal

Benoit Guizard

Hicham Maskrot

Nathalie Herlin-Boime

Dominique Porterat

Disclosed is a method for producing particles, including the steps: introducing, into a reaction chamber, at least one reaction flow including a first chemical element and propagating in a direction of flow; projecting a radiation beam through the reaction chamber, intersecting each reaction stream in one interaction area per reaction flow, to form, in each reaction flow, particle cores including the first chemical element; and introducing, into the reaction chamber, a second chemical element interacting with each reaction flow to cover the particle cores with a layer including the second chemical element. Each reaction flow is preferably free of any agent oxidizing the first chemical element. Preferably a ratio of one atom of the second element is introduced per unit of time for at least two atoms of the first element introduced per unit of time. The second element is preferably introduced in at least one confined flow.

Method for producing multilayer submicron particles by laser pyrolysis

A container with improved sealing, for improved security in the event of loading, transporting and/or unloading submicron particles, in particular nanopowder/nanoparticles, includes a connector for injecting liquid and/or gas. Such a container can also contain at least one inflatable seal () valve (). The container is provided with elements for changing the physical state of the material by heating, mixing or ultrasound bombardment. A method for using the container and an inflatable seal valve are also described.

Valve and sealed container for submicron particles, and method for using same

A method is followed to prepare a powder that includes carbon, silicon and boron, the silicon being in silicon carbide form and the boron being in boron carbide and/or free boron form. The method includes contacting a carbon-based precursor, a silicon-based precursor and a boron-based precursor BX3, X being a halogen atom, to obtain a mixture of these three precursors. The resulting mixture is subjected to laser pyrolysis. The boron-based precursor BX3 is heated, prior to the contacting step and/or simultaneously with the contacting step, to a temperature higher than the condensation temperature of the precursor.

Method for preparing a powder comprising carbon, silicon and boron, the silicon being in silicon carbide form and the boron being in boron carbide form and/or boron alone

A system and process for production of nanometric or sub-micrometric powders in continuous flux under the action of laser pyrolysis in at least one interaction zone between a beam emitted by a laser and a flux of reagents emitted by an injector, in which the laser is followed by optical means for distributing the energy of the beam emitted by the latter according to an axis perpendicular to the axis of each flux of reagents, in an elongated cross-section having adjustable dimensions at the level of this at least one interaction zone.

Production of nanometric or sub-micrometric powders in continuous flux

The invention relates to a gas phase method for producing nanometric particles in a reactor for producing particles in a gas phase, in which there is an interaction between a reaction flow and an energy flow. This method comprises the following steps: a step for coupling a device for producing gaseous chlorides with this reactor, a step for producing gaseous chlorides from a base precursor in the form of powders, and a step for injecting such a reaction flow into the reactor.

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Paris, France

Francois Tenegal