Institut Francais Du Pe'trole

Other

François Couillard

Daniel Durand

Alain Foucault

The invention relates to a method for separating constituents of a liquid feed by liquid-liquid centrifugal chromatography and to a device for implementing it. Constituents (A, B) having different partition coefficients such that they are respectively carried along at unequal velocities by a light solvent (l) and a heavier solvent (L), the feed is continuously injected at an intermediate point of a separation column (col), successive cycles comprising alternately a heavy solvent injection stage and a light solvent injection stage are carried out respectively at the two ends of the column consisting of the interconnection in series of at least one set of separation cells, and the separated solvents (FA, FB) are collected during each one of said stages at the column ends opposite the solvent injection points.

Method and device for separating constituents of a liquid feed by liquid-liquid centrifugal chromatography

The invention relates to a method for separating constituents of a liquid feed by liquid-liquid centrifugal chromatography and to a device for implementing it. Constituents (A, B) having different partition coefficients such that they are respectively carried along at unequal velocities by a light solvent () and a heavier solvent (L), the feed is continuously injected at an intermediate point of a separation column (col), successive cycles comprising alternately a heavy solvent injection stage and a light solvent injection stage are carried out respectively at the two ends of the column consisting of the interconnection in series of at least one set of separation cells, and the separated solvents (FA, FB) are collected during each one of said stages at the column ends opposite the solvent injection points.

Method and device for separating constituents of a liquid charge by means of liquid-liquid centrifuge chromatography

A method and system is intended for fine proportioning of fluids injected into a pumping installation, e.g., a liquid chromatography installation, allowing to compensate for non-return valve errors. The system includes a fluid delivery system including vessels for constituents (A, B, X) that communicate with a pumping unit () by means of a one-way valve () that opens upon suction, and a control unit (PC) that adjusts the respective proportions of the various fluids sucked by acting on the opening time of solenoid valves (EVto Even) associated with the various vessels. As the opening and closing times of the one-way valve are most often unequal in practice, control unit (PC) is suited to cyclically change the order of the control signals applied to the various solenoid valves during the various successive suction stages of each pumping unit so as to compensate on average for the proportioning inequalities due to each one-way valve.

Growing community of inventors

56860 Sene, France

François Couillard