Leybold-heraeus Gmbh

Fernand Kuhlmann

Franz Hugo

Erwin Wanetzky

The invention concerns a method, equipment and a regulating means for use in recovering metal-carbide scrap by alloying. This is carried out by treating the scrap with a low melting point metal which brings the metal-carbide matrix into solution at temperature above the melting point of the alloy formed. The treatment is carried out in a container in the presence of inert gas, the pressure of which is gradually reduced following completion of the alloying process, the resultant metal vapor being condensed. To solve the problem of producing, in the resultant residue, a proportion of low melting point metal of less than 100 ppm and of preventing condensation of the metal vapors on the container, it is proposed in the invention that the metal-carbide scrap and the low melting point metal should be alloyed with each other in an inner chamber arranged within the container. The metal vapor and the inert gas are passed out of this inner chamber on to the condensation surfaces, and the inert gas, containing no metal vapors, is cycled by way of the inner chamber. The metal vapor then serves as a means for inducing flow of the inert gas.

Equipment and regulating means for recovering metal-carbide scrap by

The invention concerns a method, equipment and a regulating means for use in recovering metal-carbide scrap by alloying. This is carried out by treating the scrap with a low melting point metal which brings the metal-carbride matrix into solution at temperatures above the melting point of the alloy formed. The treatment is carried out in a container in the presence of inert gas, the pressure of which is gradually reduced following completion of the alloying process, the resultant metal vapor being condensed. To solve the problem of producing, in the resultant residue, a proportion of low melting point metal of less than 100 ppm and of preventing condensation of the metal vapors on the container, it is proposed in the invention that the metal-carbide scrap and the low melting point metal should be alloyed with each other in an inner chamber arranged within the container. The metal vapor and the inert gas are passed out of this inner chamber on to the condensation surfaces, and the inert gas, containing no metal vapors, is cycled by way of the inner chamber. The metal vapor then serves as a means for inducing flow of the inert gas.

Method for recovering metal-carbide scrap by alloying

The invention relates to a distillation and sublimation apparatus having a receiving vessel and a number of containers for the starting product. Each container has a bottom, an outer wall and an inner wall with a vapor duct, and the containers are stacked one upon the other in such manner that the vapor ducts are arranged in series. An annular space is present outside the stack of containers. The apparatus comprises a condenser into which the vapor duct of the bottom container discharges. For the purpose of solving the problem of preventing condensation of vapor on the receiving vessel, it is proposed, in accordance with the invention, that capillary gaps (28), which are open towards the receiving vessel (3), be present between the containers (26). Furthermore, the condenser (8) communicates with the annular space (10) by way of at least one return-flow orifice (19) for the gases. The arrangement is such that the annular space (10), the capillary gaps (28), the vapor ducts (26), the condenser (8) and the return-flow orifice or orifices (19) are parts of a closed gas-circulation path.

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Seligenstadt, Germany

Fernand Kuhlmann