Ahlstrom Machinery Oy

A. Ahlstrom Corporation

Erik Agren

Olof Fagerlind

Krister Sannholm

Ake Schonberg

Juhani Hoikkala

Falling film evaporator

A method and an apparatus are provided for controlling crystallization (and thus preventing harmful fouling of heat transfer surfaces) during the treatment of black liquor. The black liquor is concentrated to a high dry solids content (at least about 70%, e.g. about 75-90%) in a falling film crystallizing apparatus (e.g. falling film evaporator). A part of the liquor flowing from the heat transfer surfaces and collected in a retention vessel (e.g. an interior volume of the evaporator) is recirculated to the heat exchange surfaces and a part of the liquor is discharged for further treatment (e.g. combustion in a recovery boiler). A part of the black liquor in the recirculation system is returned directly to the retention vessel in order to facilitate mixing and thus to bring about, in the retention vessel, crystallization of inorganic salts of the black liquor that is as complete as possible. Some of the discharged black liquor also may be returned, and a mixer and/or baffles disposed in the retention tank, to further enhance mixing.

Method and apparatus for treatment of black liquor

A process and apparatus provide for the evaporation of spent liquors in several stages, and recovery of volatile substances from spent liquors of organic solvent pulping processes. The recovery system for volatiles is integrated with the evaporation of spent liquors. Heating condensation is carried out in each evaporator effect on several heat surfaces separated from each other. Pure water, vapor condensate, or steam may be injected to the warmer side of an evaporator effect in order to increase the condensing temperature of the vapor. The volatiles are typically alcohols (methanol and/or ethanol) used as the cooking liquor in organic solvent pulping.

Process for the concentration of spent liquors

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Esbo, Finland

Erik Agren