E.i. Dupont De Nemours and Company

Edgar W Slocum

Robert Clayton Wheland

Ashok H Shah

Arthur William Etchells

Aquiles C Sobrero

Don Mayo Coates

Tom Edward Estep

Charles Wesley Starke

Robert E Albers

Joseph Daniel Gutmann, Jr

This invention relates to mixing two substantially immiscible fluids having substantial viscosity differences into a single phase solution. The invention particular includes a mixer comprising a specially designed conveyor flights to provide shear mixing without differential conveying of the fluids or causing excessive back pressure or pressure drop on the solution.

Forming a solution of fluids having low miscibility and large-scale differences in viscosity

A mixing apparatus for continuously generating a homogeneous mixture of a polymer and a less viscous fluid is provided. The mixer includes means for continuously injecting a viscous polymer into a pressure vessel; means for continuously injecting a lower viscosity fluid into the pressure vessel; means for continuously injecting a plasticizing agent into the viscous polymer entering the pressure vessel; high shear centrifugal mixing means within the pressure vessel for mixing the polymer and the less viscous fluid; drive means for rotating the rotational mixing means; heating means for maintaining the temperature of the substances being mixed in the pressure vessel at a desired mixing temperature; and means for continuously discharging a homogeneous mixture of the polymer, the plasticizing agent, and the less viscous fluid from the mixer.

Process and apparatus for mechanically mixing polymers and lower

A free-radical initiated process for preparing fluorinated polymers wherein at least one gaseous fluoroolefin is polymerized in a stirred polymerizer, the improvement comprising preparing a non-volatile polymeric seed in a reaction zone separate from the polymerizer by decomposing initiator in the presence of fluoromonomer to form oligomeric free radicals and condensing said radicals onto previously prepared polymer; and conveying said non-volatile seed to the polymerizer.

Polymerization of fluoroolefins in presence of non-volatile polymeric

The polymerization of fluoromonomers can be accomplished without fouling by using gaseous monomers in the presence of at least one nonvolatile initiator and by recycling the initiator-free polymerizer gases through an external cooler.

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Wilmington, DE, United States of America

Edgar W Slocum