Bayer Aktiengesellschaft

Chemische Werke Huls Aktiengesellschaft

Bunawerke Huls Gmbh

Bunkawerke Huls Gmbh

Eckhard Moller

Edgar Muschelknautz

Roland Vogelsgesang

Bernhard Schleimer

Walter Breuker

Bernt Kesper

Hans Wagner

Karl-Heinz Magosch

Helmut Ohse

Hans Westermann

Wilhelm Schiemann

Klaus Hachmann

Horst-Dieter Bures

This invention concerns a method for precipitating polymers from a liquid using at least one precipitant fluid, including a feed line, a nozzle plate having at least one outlet orifice for a polymer containing fluid with the outlet orifice communicating with the feed line, at least one nozzle for at least one precipitant fluid, the axis of which is arranged approximately perpendicularly to the axis of the outlet orifice, a precipitation chamber positioned on the side of the nozzle plate wherein at least one nozzle for at least one precipitant fluid is located, a discharge line for discharging a mixture which contains the precipitated polymer and a degassing chamber which is connected to the discharge line.

Process for precipitating polymers

A device for precipitating polymers from a liquid by at least one precipitant fluid includes a feed line, a nozzle plate having at least one outlet orifice for a polymer containing fluid with the outlet orifice communicating with the feed line, at least one nozzle for at least one precipitant fluid, the axis of which is arranged approximately perpendicularly to the axis of the outlet orifice, a precipitation chamber positioned on the side of the nozzle plate wherein at least one nozzle for at least one precipitant fluid is located, a discharge line for discharging a mixture which contains the precipitated polymer and a degassing chamber which is connected to the discharge line.

Device and process for precipitating polymers

A flow-promoting device in combination with a heated box tray open at the top in a reaction and degasification column in which a viscous or highly viscous liquid is flowing from an inlet end to an outlet end of the tray and in which a heating tube register is located to be completely covered by the liquid. The tube register includes a plurality of heating tubes spaced from each other, and the flow-promoting device has a bottom heating unit for the box tray positioned outside and along the bottom of the tray, a siphon plate mounted on the tray at a liquid inlet end of the tray and closely in front of the tube register, with the siphon plate having a bottom end extending to the underside of the tube register, and a weir positioned at the liquid outlet end of the box tray. The weir has a top edge extending at least to the topside of the tube register, and the spacing of the weir from the tube register is larger than the spacing of the siphon plate at the inlet end from the tube register.

Open heated box trays having flow-promoting devices

In the production of polyesters by introduction of precondensates on to a first plate of a column reactor product quality is improved and operating time is increased in that spontaneous flash evaporation of the precondensate takes place in a so-called entry box, before the introduction on to the first plate of the column reactor, and in that separation of the liquid component from the gaseous component is subsequently carried out by centrifugal force in a so-called annular chamber.

Process for the production of polyesters

Growing community of inventors

Marl, Germany

Eckhard Moller