Council of Scientific and Industrial Research

Deepti Mishra

Sudhir Sitaram Amritphale

Barada Kanta Mishra

Satyabrata Das

Mohammed Akram Khan

Avneesh Anshul

Ramesh Kumar Chouhan

Manish Mudgal

Archana Singh

Navin Chandra

Swati Lahiri

The present invention provides a nano phosphatic hybrid geopolymeric corrosion resistant coating material. The tailored precursor of corrosion resistant coating material is obtained by a process involving, together dry grinding of raw materials fly ash, sodium hydroxide, rice husk, tri calcium phosphate and cetyl trimethyl ammonium bromide optionally with sodium silicate, in solid powder form. The developed coating material obtained by adding water to tailored precursor contains nano sized phosphatic compounds of Cancrisilite (sodium aluminum carbonate silicate hydrate), quartz, mullite, heamatite, sodium aluminum silicate, Herschelite (sodium aluminum silicate hydrate), Sucrose, &#x3b1; D-Glucose, Native cellulose, and phenol, responsible for providing improved corrosion resistant properties and adhesion to the mild steel substrates. The geo-polymeric coating material is used as an anti-corrosive, heat resistant coating material on various materials e.g. mild steel substrates.

Nano phosphatic hybrid geopolymeric corrosion resistant coating material and a method of preparation thereof

The present invention provides a composition for advanced hybrid geopolymeric functional materials possessing very broad application spectrum ranging from cementitious materials to advanced functional materials having 'Inorganic-Organic Hybrid' matrix in contrast to the limited application of conventional geopolymeric materials having 'Inorganic matrix' only. The invention further relates to a process for the preparation of these materials. The process obviates the need of external addition of sodium silicate which is one of the costliest and main raw materials in conventional geopolymerisation processes. Interestingly, in the present invention the sodium silicate has been synthesized in situ by designing of conditions for synergistic and simultaneous mechano-chemical reactions among the selected raw materials viz. inorganic and organic wastes under alkaline environment. This results in the formation of &#x201c;Hybrid inorganic-organic frame work&#x201d; of sodium silicate, which facilitates uniform dispersion of reacting species, thus resulting in the formation of homogeneous geopolymeric matrix with improved characteristics.

Composition for advanced hybrid geopolymeric functional materials and a process for the preparation thereof

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Madhya Pradesh, India

Deepti Mishra