Inco Limited

David E Hall

Samuel W Marcuson

Carlos A Landolt

Robert C Francki

The invention relates to the smelting or converting of particulate sulfide material, such as nickel or copper sulfide. A molten seed bath of smelted or converted material is provided in a reaction vessel. Particulate sulfide material is injected into a reaction vessel below the surface of the melt. Top blowing with an oxygen-containing gas generates heat and brings about the oxidation of the sulfides with a significant decrease in the amount of dust generated. Optional bottom stirring with a non-reactive gas such as nitrogen may further increase efficiency.

Conversion of non-ferrous sulfides

A non-ferrous matte conversion process is disclosed in which molten non-ferrous matte, essentially nickel and/or copper sulfide and iron sulfide, is provided in a suitable vessel, such as a modified Pierce-Smith converter. The bath is stirred from below with a non-reactive sparging gas, such as nitrogen, and surfaceblown from above with an oxygen-containing gas. A flux is added to the melt to raise a fluid slag. In addition, cold crushed matte is added to the bath. The cold matte acts to maintain the temperature of the bath, so as to prevent overheating which can damage the converter lining. The matte addition also serves as a source for additional converter feed. As the reaction progresses, the slag layer is periodically skimmed, and additions of flux and cold matte are made when necessary. When it is no longer possible to raise a slag, a non-ferrous sulfide matte is obtained having a greatly reduced iron content.

Conversion of non-ferrous matte

An injector for introducing particulate material into the bath of a pyrometallurgical vessel via existing tuyeres. An existing mechanical puncher may be removed and replaced with an injector adapted to be attached to the existing tuyere body so as not to disturb the existing blast air connections. The injector, including a housing spatially circumscribing an injector pipe and forming an annular space part way therewith, is inserted into the tuyere. A source of pressurized fluid is injected into the annular space keeping the tuyere open so the particulate material can be introduced through the pipe.

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Sudbury, Canada

David E Hall