Battelle Memorial Institute

Revive Environmental Technology, LLC

Darwin Argumedo

Slawomir Winecki

Joshua James

Joseph Casciano

Michael M Miller

Jeffrey L Ellis

Rachid Taha

David Arthur Holley

Kavitha Dasu

Christopher Gordon Scheitlin

Lindy E Dejarme

Vinay V Gadkari

Aaron Frank

Rick Peterson

Doug Hendry

Keith Brown

Michael Heinrichs

Dan Garbark

Nathan Bryant

Keith E Brown

Ian Haggerty

Kurt Blohm

Ann E Lane

Patrick Norris

Richard Peterson

Vivek Lal

John Tallarico

Tom McGuinness

Douglas Hendry

Stephen H Rosansky

Russell R Sirabian

Russel R Sirabian

Haskell Jac Fought

Meghan Harley Yugulis

Robert Stonebraker

William Gibbs

Amy M Heintz

John P Tallarico

Christopher F Buurma

Matthew Vaughan

Michael Miller

Amy Dindal

Meghan Harley Yugulus

Per- and polyfluoroalkyl substances (PFAS) are destroyed by oxidation in supercritical conditions. PFAS in water is concentrated in a reverse osmosis step and salt from the resulting solution is removed in supercritical conditions prior to destruction of PFAS in supercritical conditions.

Salt separation and destruction of PFAS utilizing reverse osmosis and salt separation

Per- and polyfluoroalkyl substances (PFAS) are destroyed by oxidation in supercritical conditions. PFAS in water can be concentrated and prepared for destruction in a pretreatment phase. Following annihilation of the PFAS in supercritical conditions to levels below 5 parts per trillion (ppt), the water effluent can be used to recover heat, returned to sub-critical conditions, and then released back into the environment.

Destruction of PFAS via an oxidation process and apparatus suitable for transportation to contaminated sites

Systems and processes for purifying and concentrating a liquid feed stream are disclosed. In the systems, the concentrated liquid output from the high pressure side of a reverse osmosis stage is used as the draw solution in the low pressure side of the reverse osmosis stage in a configuration called osmotically assisted reverse osmosis. This reduces the osmotic pressure differential across the membrane, permitting high solute concentrations to be obtained, hastening the purification of the liquid. Reduced system pressures are also obtained by arranging multiple osmotically assisted reverse osmosis stages in a cross-current arrangement. Overall system energy consumption is reduced compared to conventional thermal processes for high concentration streams.

Cross current staged reverse osmosis

A system for recovering rare earth elements from coal ash includes a leaching reactor, an ash dryer downstream of the leaching reactor, and a roaster downstream of the ash dryer that is cooperatively connected to both the leaching reactor and the ash dryer. Coal ash is mixed with an acid stream such that rare earth elements present in the coal ash are dissolved in the acid stream, thereby creating (i) a leachate containing the rare earth elements and (ii) leached ash. The leachate is heated to obtain acid vapor and an acid-soluble rare earth concentrate. Mixing of the coal ash with the acid stream can occur in a leaching reactor and heating of the leachate can occur in a roaster. The acid-soluble rare earth concentrate can be fed to a hydrometallurgical process to separate and purify the rare earth elements.

Systems for acid digestion processes

Methods of recovering rare earth elements, vanadium, cobalt, or lithium from coal are described. The coal is dissolved in a first solvent to dissolve organic material in the coal and create a slurry containing coal ash enriched with rare earth elements, vanadium, cobalt, or lithium. The enriched coal ash is separated from the first solvent. Residual organic material is removed from the coal ash. The rare earth elements, vanadium, cobalt, or lithium can then be recovered from the coal ash. The coal ash is mixed with an acid stream that dissolves the rare earth elements, thereby creating (i) a leachate containing the rare earth elements and (ii) leached ash. The leachate is heated to obtain acid vapor and an acid-soluble rare earth concentrate. The acid-soluble rare earth concentrate can be fed to a hydrometallurgical process to separate and purify the rare earth elements.

Methods for recovery of rare earth elements from coal

A method of making a zeolite comprises: adding a zeolite seed to a leach solution containing silicon and aluminum; and heating the leach solution to obtain the zeolite. The leach solution can be made by mixing coal ash with a basic stream, thereby creating (i) a leach solution containing silicon and aluminum, and (ii) leached ash; and separating the leach solution from the leached ash.

Methods for making zeolites

Acid digestion processes for recovery of rare earth elements from coal and coal byproducts

The present disclosure relates to systems and methods for measuring oil/water content in oil-water mixtures, regardless of the salinity of the mixture. The oil content is measured using a dielectric sensor. It is determined whether the oil content is above or below a threshold. If the oil content is above the threshold, the oil content is reported using the measurement from the dielectric sensor. If the oil content is below the threshold, the oil content is reported using the measurement from the eddy current sensor.

Oil recovery sensor

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Columbus, OH, United States of America

Darwin Argumedo