Ut-battelle, Inc.

Honeywell International Inc.

Dane Francis Wilson

David Eugene Holcomb

Govindarajan Muralidharan

Sunil K Menon

George Daniel Hadden

Gary Scott Whittaker

Russell D Braunling

Weiju Ren

A method of stripping tritium from flowing stream of molten salt includes providing a tritium-separating membrane structure having a porous support, a nanoporous structural metal-ion diffusion barrier layer, and a gas-tight, nonporous palladium-bearing separative layer, directing the flowing stream of molten salt into contact with the palladium-bearing layer so that tritium contained within the molten salt is transported through the tritium-separating membrane structure, and contacting a sweep gas with the porous support for collecting the tritium.

Apparatus and method for stripping tritium from molten salt

An essentially Fe-free alloy consists essentially of, in terms of weight percent: 4 to 11 Co, 6.5 to 7.5 Cr, 0 to 0.15 Al, 0.5 to 0.85 Mn, 11 to 20 Mo, 1 to 3.5 Ta, 0.05 to 9 W, 0.03 to 0.08 C, 0 to 0.001 B, 0.0005 to 0.005 N, balance Ni, the alloy being characterized by, at 850&#xb0; C., a yield strength of at least 25 Ksi, a tensile strength of at least 45 Ksi, a creep rupture life at 12 Ksi of at least 10 hours, and a corrosion rate, expressed in weight loss [g/(cmsec)]10during a 1000 hour immersion in liquid FLiNaK at 850&#xb0; C., in the range of 5 to 20.

Creep-resistant, cobalt-containing alloys for high temperature, liquid-salt heat exchanger systems

An alloy is composed essentially of, in terms of weight percent: 6 to 8.5 Cr, 5.5 to 13.5 Mo, 0.4 to 7.5 W, 1 to 2 Ti, 0.7 to 0.85 Mn, 0.05 to 0.3 Al, 0.08 to 0.5 C, 0 to 1 Nb, with the balance Ni, the alloy being characterized by, at 850&#xb0; C., a yield strength of at least 25 Ksi, a tensile strength of at least 30 Ksi, a creep rupture life at 12 Ksi of at least 45 hours, and a corrosion rate, expressed in weight loss [g/(cmsec)]10during a 1000 hour immersion in liquid FLiNaK at 850&#xb0; C., in the range of 6 to 39.

Intermediate strength alloys for high temperature service in liquid-salt cooled energy systems

An alloy consists essentially of, in terms of weight percent: 6 to 8.5 Cr, 5.5 to 13.5 Mo, 0.4 to 7.5 W, 1 to 2 Ti, 0.7 to 0.85 Mn, 0.05 to 0.3 Al, up to to 0.1 Co, 0.08 to 0.5 C, 1 to 5 Ta, 1 to 4 Nab, 1 to 3 Hf, balance Ni. The alloy is characterized by, at 850&#xb0; C., a yield strength of at least 36 Ksi, a tensile strength of at least 40 Ksi, a creep rupture life at 12 Ksi of at least 72.1 hours, and a corrosion rate, expressed in weight loss [g/(cm2sec)]&#xd7;10during a 1000 hour immersion in liquid FLiNaK at 850&#xb0; C., in the range of 8 to 25.

An essentially cobalt-free alloy consists essentially of, in terms of weight percent: 6.3 to 7.2 Cr, 0.5 to 2 Al, 0 to 5 Fe, 0.7 to 0.8 Mn, 9 to 12.5 Mo, 0 to 6 Ta, 0.75 to 3.5 Ti, 0.01 to 0.25 Nb, 0.2 to 0.6 W, 0.02 to 0.04 C, 0 to 0.001 B, 0.0001 to 0.002 N, balance Ni. The alloy is characterized by a &#x3b3;' microstructural component in the range of 3 to 17.6 weight percent of the total composition. The alloy is further characterized by, at 850&#xb0; C., a yield strength of at least 60 Ksi, a tensile strength of at least 70 Ksi, a creep rupture life at 12 Ksi of at least 700 hours, and a corrosion rate, expressed in weight loss [g/(cmsec)]10during a 1000 hour immersion in liquid FLiNaK at 850&#xb0; C., in the range of 5.5 to 17.

High strength alloys for high temperature service in liquid-salt cooled energy systems

An essentially Fe- and Co-free alloy is composed essentially of, in terms of weight percent: 6.0 to 7.5 Cr, 0 to 0.15 Al, 0.5 to 0.85 Mn, 11 to 19.5 Mo, 0.03 to 4.5 Ta, 0.01 to 9 W, 0.03 to 0.08 C, 0 to 1 Re, 0 to 1 Ru, 0 to 0.001 B, 0.0005 to 0.005 N, balance Ni, the alloy being characterized by, at 850&#xb0; C., a yield strength of at least 25 Ksi, a tensile strength of at least 38 Ksi, a creep rupture life at 12 Ksi of at least 25 hours, and a corrosion rate, expressed in weight loss [g/(cmsec)]10during a 1000 hour immersion in liquid FLiNaK at 850&#xb0; C., in the range of 3 to 10.

Creep-resistant, cobalt-free alloys for high temperature, liquid-salt heat exchanger systems

Disclosed herein are systems, devices and methods for stress-rupture testing selected materials within a high-temperature liquid salt environment. Exemplary testing systems include a load train for holding a test specimen within a heated inert gas vessel. A thermal break included in the load train can thermally insulate a load cell positioned along the load train within the inert gas vessel. The test specimen can include a cylindrical gage portion having an internal void filled with a molten salt during stress-rupture testing. The gage portion can have an inner surface area to volume ratio of greater than 20 to maximize the corrosive effect of the molten salt on the specimen material during testing. Also disclosed are methods of making a salt ingot for placement within the test specimen.

Liquid salt environment stress-rupture testing

A corrosion sensor and method for its use to detect and determine the, type, location, size and growth rate of corrosion of metals and the like in a corrosive environment. The corrosion sensor can distinguish between different types of corrosion such as uniform corrosion, pitting, crevice, and stress corrosion cracking. The sensor detects corrosion conditions of a corrodible metal article in a corrosive environment. It has a metal probe comprised of a metal which is substantially identical to that of the corrodible metal article and a transducer element attached to said probe, which is capable of projecting and receiving ultrasonic or radio frequency signals through the probe. The received signals indicate corrosion of the probe and hence the corrodible metal article.

Growing community of inventors

Oak Ridge, TN, United States of America

Dane Francis Wilson